ChemicalBook > CAS DataBase List > 4-IODOPHTHALONITRILE 97
4-IODOPHTHALONITRILE 97
- Product Name
- 4-IODOPHTHALONITRILE 97
- CAS No.
- 69518-17-8
- Chemical Name
- 4-IODOPHTHALONITRILE 97
- Synonyms
- 4-Iodophthalonitri;4-Iodophthalonitrile 97%;4-IODOPHTHALONITRILE 97;1,2-Dicyano-4-iodobenzene;1,2-Benzenedicarbonitrile, 4-iodo-
- CBNumber
- CB2499525
- Molecular Formula
- C8H3IN2
- Formula Weight
- 254.03
- MOL File
- 69518-17-8.mol
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4-IODOPHTHALONITRILE 97 Property
- Melting point:
- 140-142 °C (lit.)
- Boiling point:
- 364.7±37.0 °C(Predicted)
- Density
- 1.95±0.1 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- form
- powder to crystaline
- color
- Light yellow to Brown
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Safety
- Hazard Codes
- Xn
- Risk Statements
- 20/21/22-36/37/38
- Safety Statements
- 26-36
- WGK Germany
- 3
- HS Code
- 2926.90.4801
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
Sigma-Aldrich
- Product number
- 515426
- Product name
- 4-Iodophthalonitrile
- Purity
- 97%
- Packaging
- 1g
- Price
- $152
- Updated
- 2024/03/01
TCI Chemical
- Product number
- I1050
- Product name
- 4-Iodophthalonitrile
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $146
- Updated
- 2024/03/01
TRC
- Product number
- I737185
- Product name
- 4-Iodophthalonitrile
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
TRC
- Product number
- I737185
- Product name
- 4-Iodophthalonitrile
- Packaging
- 500mg
- Price
- $200
- Updated
- 2021/12/16
AK Scientific
- Product number
- 1633BB
- Product name
- 4-Iodophthalonitrile
- Packaging
- 1g
- Price
- $224
- Updated
- 2021/12/16
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4-IODOPHTHALONITRILE 97 Chemical Properties,Usage,Production
Synthesis
1.6 g (0.011 mol) 4-aminophthalonitrile was dissolved in 22.4 mL of 2.5 M
H2SO4. The mixture was cooled to 0 ??C. To the solution was slowly added 0.9 g
(0.013 mol) of NaNO2 dissolved in 3.5 mL of water. After the mixture was stirred for
30 minutes, 2.08 g (0.013 mol) of KI dissolved in 12.8 mL of water was added. The
mixture was further stirred for 45 minutes at room temperature. After this period, the
brown solid was filtered and washed with water. It was dissolved in a minimal
amount of chloroform. The solution was washed first with saturated Na2S2O3 and
then with water. It was dried over Na2SO4. After the solution was filtered, it was
dried in vacuum and purified with column chromatography over silica gel by eluting
with dichloromethane. Molecular formula: IC6H3-1,2-(CN)2 (254.03 g/mol). Yield:
2.37 g (85%).
4-IODOPHTHALONITRILE 97 Preparation Products And Raw materials
Raw materials
Preparation Products
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