ChemicalBook > CAS DataBase List > 2 3 4-(TRIMETHOXY)BROMOBENZENE 99

2 3 4-(TRIMETHOXY)BROMOBENZENE 99

Product Name
2 3 4-(TRIMETHOXY)BROMOBENZENE 99
CAS No.
10385-36-1
Chemical Name
2 3 4-(TRIMETHOXY)BROMOBENZENE 99
Synonyms
1-Bromo-2,3,4-trimethoxybenzene;Benzene,1-bromo-2,3,4-trimethoxy-;2 3 4-(TRIMETHOXY)BROMOBENZENE 99
CBNumber
CB2504810
Molecular Formula
C9H11BrO3
Formula Weight
247.09
MOL File
10385-36-1.mol
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2 3 4-(TRIMETHOXY)BROMOBENZENE 99 Property

Boiling point:
105-110 °C/2 mmHg (lit.)
Density 
1.291 g/mL at 25 °C (lit.)
refractive index 
n20/D 1.549(lit.)
Flash point:
>230 °F
storage temp. 
2-8°C
Appearance
Light yellow to yellow Liquid
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Safety

WGK Germany 
3
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
554111
Product name
2,3,4-(Trimethoxy)bromobenzene
Purity
99%
Packaging
1g
Price
$72.5
Updated
2023/01/07
TRC
Product number
B701205
Product name
1-Bromo-2,3,4-trimethoxybenzene
Packaging
100mg
Price
$60
Updated
2021/12/16
AK Scientific
Product number
J53328
Product name
1-Bromo-2,3,4-trimethoxybenzene
Packaging
10g
Price
$320
Updated
2021/12/16
AK Scientific
Product number
J53328
Product name
1-Bromo-2,3,4-trimethoxybenzene
Packaging
25g
Price
$640
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0066933
Product name
2,3,4-(TRIMETHOXY)BROMOBENZENE
Purity
95.00%
Packaging
1G
Price
$673.32
Updated
2021/12/16
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2 3 4-(TRIMETHOXY)BROMOBENZENE 99 Chemical Properties,Usage,Production

General Description

2,3,4-(Trimethoxy)bromobenzene can be prepared from 1,2,3-(trimethoxy)benzene via bromination.

Synthesis

634-36-6

10385-36-1

General procedure for the synthesis of 2,3,4-tris(methoxy)bromobenzene from 1,2,3-trimethoxybenzene: In a dry 45 mL reaction tube equipped with a magnetic stirrer (note: the air inside the reaction tube is not displaced), 1 mL of [Bmim]NO3 as solvent, 0.5 mmol of 1,2,3-trimethoxybenzene, and 0.25 mmol of Br2 were added. The reaction tube was then sealed and the reaction was stirred at 80 °C for 24 hours. Upon completion of the reaction, the mixture was cooled to room temperature and diluted with 3 mL of water. The reaction mixture was extracted with dichloromethane (3 x 10 mL) to isolate the target product 2,3,4-tris(methoxy)bromobenzene. The GC yield of the product was determined by gas chromatography (GC) analysis. In another parallel experiment, the product was purified by column chromatography and structurally characterized using 1H NMR and 13C NMR.

References

[1] Synthetic Communications, 2007, vol. 37, # 2, p. 323 - 328
[2] Australian Journal of Chemistry, 1992, vol. 45, # 12, p. 1967 - 1982
[3] Journal of Chemical Research - Part S, 1998, # 10, p. 662 - 663
[4] Russian Journal of Organic Chemistry, 2007, vol. 43, # 9, p. 1282 - 1284
[5] Synthetic Communications, 2005, vol. 35, # 14, p. 1947 - 1952

2 3 4-(TRIMETHOXY)BROMOBENZENE 99 Preparation Products And Raw materials

Raw materials

Preparation Products

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2 3 4-(TRIMETHOXY)BROMOBENZENE 99 Suppliers

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View Lastest Price from 2 3 4-(TRIMETHOXY)BROMOBENZENE 99 manufacturers

R&D Scientific Inc.
Product
1-Bromo-2,3,4-trimethoxybenzene 10385-36-1
Price
US $350.00/g
Min. Order
1g
Purity
97
Supply Ability
500 Kg
Release date
2024-03-27

10385-36-1, 2 3 4-(TRIMETHOXY)BROMOBENZENE 99Related Search:

2 3 4-(TRIMETHOXY)BROMOBENZENE 99 AURORA 7596 AURORA 5734 AURORA 8292 AURORA 5315 AURORA 8249 AURORA 5350 AURORA 4592 AURORA 8149 AURORA 23145 AURORA 4601 AURORA 5246 AURORA 6715 AURORA 2022 AURORA 4591 AURORA 7667 AURORA 4593 AURORA 5245

  • Benzene,1-bromo-2,3,4-trimethoxy-
  • 1-Bromo-2,3,4-trimethoxybenzene
  • 2 3 4-(TRIMETHOXY)BROMOBENZENE 99
  • 10385-36-1
  • BrC6H2OCH33
  • Ethers
  • Organic Building Blocks
  • Oxygen Compounds