3-(2-DIMETHYLAMINOETHOXY)-BROMOBENZENE
- Product Name
- 3-(2-DIMETHYLAMINOETHOXY)-BROMOBENZENE
- CAS No.
- 221915-84-0
- Chemical Name
- 3-(2-DIMETHYLAMINOETHOXY)-BROMOBENZENE
- Synonyms
- UKRORGSYN-BB BBV-070799;3-(2-DIMETHYLAMINOETHOXY)-BROMOBENZENE;2-(3-BroMophenoxy)-N,N-diMethylethanaMine;[2-(3-BROMO-PHENOXY)-ETHYL]-DIMETHYL-AMINE;2-(3-bromophenoxy)-n,n-dimethylethan-1-amine;Ethanamine, 2-(3-bromophenoxy)-N,N-dimethyl-
- CBNumber
- CB2691961
- Molecular Formula
- C10H14BrNO
- Formula Weight
- 244.13
- MOL File
- 221915-84-0.mol
3-(2-DIMETHYLAMINOETHOXY)-BROMOBENZENE Property
- Boiling point:
- 280.0±20.0 °C(Predicted)
- Density
- 1.309±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 8?+-.0.28(Predicted)
- Appearance
- Colorless to light yellow Liquid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H318Causes serious eye damage
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B700923
- Product name
- 2-(3-Bromophenoxy)-N,N-dimethylethanamine
- Packaging
- 500mg
- Price
- $155
- Updated
- 2021/12/16
- Product number
- 5205AJ
- Product name
- 2-(3-Bromophenoxy)-N,N-dimethylethanamine
- Packaging
- 1g
- Price
- $173
- Updated
- 2021/12/16
- Product number
- 150521
- Product name
- 2-(3-Bromophenoxy)-N,N-dimethylethanamine
- Purity
- 95%
- Packaging
- 1g
- Price
- $278
- Updated
- 2021/12/16
- Product number
- HCH0056165
- Product name
- [2-(3-BROMOPHENOXY)ETHYL]DIMETHYLAMINE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $808.89
- Updated
- 2021/12/16
- Product number
- 150521
- Product name
- 2-(3-Bromophenoxy)-N,N-dimethylethanamine
- Purity
- 95%
- Packaging
- 5g
- Price
- $861
- Updated
- 2021/12/16
3-(2-DIMETHYLAMINOETHOXY)-BROMOBENZENE Chemical Properties,Usage,Production
Synthesis
108-01-0
591-20-8
221915-84-0
Diisopropyl diisopropyl diisopropyl-1,2-dicarboxylate (1.56 g, 7.34 mmol) was slowly added dropwise to a solution of THF (20 mL) containing 3-bromophenol (1.155 g, 6.68 mmol), 2-(dimethylamino)ethanol (0.65 g, 7.34 mmol) and triphenylphosphine (1.93 g, 7.34 mmol) at 0 °C. The reaction mixture was gradually warmed to room temperature over a period of 16 h. The volatiles were subsequently removed by distillation under reduced pressure. The residue was dissolved in ethyl acetate (20 mL) and extracted with 1N HCl (20 mL), the aqueous phase was retained and washed with ethyl acetate. The aqueous phase was subsequently neutralized with saturated NaHCO3 solution (50 mL), extracted again with ethyl acetate, and the organic phase was dried over anhydrous MgSO4. Finally, the target product 2-(3-bromophenoxy)-N,N-dimethylethylamine (1.03 g, 63% yield) was purified by silica gel column chromatography (eluent: 4% MeOH/DCM) as an oil.
References
[1] Patent: WO2009/111279, 2009, A1. Location in patent: Page/Page column 93
3-(2-DIMETHYLAMINOETHOXY)-BROMOBENZENE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-(2-DIMETHYLAMINOETHOXY)-BROMOBENZENE manufacturers
- Product
- 3-(2-DIMETHYLAMINOETHOXY)-BROMOBENZENE 221915-84-0
- Price
- US $0.01/KG
- Min. Order
- 1KG
- Purity
- 98%; 99%
- Supply Ability
- 1kg; 10kg; 25kg
- Release date
- 2020-01-07