5-CHLORO-2,3-DIPHENYL-1H-INDOLE

Product Name: 5-CHLORO-2,3-DIPHENYL-1H-INDOLE
CAS No.: 52598-02-4
Chemical Name: 5-CHLORO-2,3-DIPHENYL-1H-INDOLE
Synonyms: 5-Chloro-2,3-diphenylindole;5-CHLORO-2,3-DIPHENYL-1H-INDOLE;1H-Indole, 5-chloro-2,3-diphenyl-
CBNumber: CB2717584
Molecular Formula: C20H14ClN
Formula Weight: 303.78
MOL File: Mol file

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5-CHLORO-2,3-DIPHENYL-1H-INDOLE Property

Melting point:: 130-131 °C(Solv: ethanol (64-17-5))
Boiling point:: 478.1±33.0 °C(Predicted)
Density: 1.243±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 15.63±0.30(Predicted)
Appearance: Light brown to brown Solid
InChI: InChI=1S/C20H14ClN/c21-16-11-12-18-17(13-16)19(14-7-3-1-4-8-14)20(22-18)15-9-5-2-6-10-15/h1-13,22H
InChIKey: BAEWCDBRAIDXMN-UHFFFAOYSA-N
SMILES: N1C2=C(C=C(Cl)C=C2)C(C2=CC=CC=C2)=C1C1=CC=CC=C1

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: C370173
Product name: 5-Chloro-2,3-diphenyl-1H-indole
Packaging: 50mg
Price: $45
Updated: 2021/12/16

TRC

Product number: C370173
Product name: 5-Chloro-2,3-diphenyl-1H-indole
Packaging: 100mg
Price: $60
Updated: 2021/12/16

Matrix Scientific

Product number: 094095
Product name: 5-Chloro-2,3-diphenyl-1H-indole
Purity: 95+%
Packaging: 250mg
Price: $265
Updated: 2021/12/16

AK Scientific

Product number: J97701
Product name: 5-Chloro-2,3-diphenyl-1H-indole
Packaging: 10g
Price: $450
Updated: 2021/12/16

Matrix Scientific

Product number: 094095
Product name: 5-Chloro-2,3-diphenyl-1H-indole
Purity: 95+%
Packaging: 1g
Price: $588
Updated: 2021/12/16

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5-CHLORO-2,3-DIPHENYL-1H-INDOLE Chemical Properties,Usage,Production

Synthesis

106-47-8

501-65-5

52598-02-4

4-Chloroaniline (76.5 mg, 0.6 mmol) and diphenylacetylene (71.3 mg, 0.4 mmol) were used as raw materials, and Cp*Rh(H2O)3(OTf)2 (11.8 mg, 5 mol%) was added to the reaction vials as a catalyst, acetic anhydride (59.0 μL, 0.6 mmol) as acylate, and 2.0 mL of tertiary amyl alcohol as the solvent. The reaction system was stirred at 100 °C for 24 h under oxygen atmosphere (1 atm). After completion of the reaction, NaOH (48 mg, 1.2 mmol) and methanol (2 mL) were added to the reaction mixture and stirring was continued for 2 hours. Subsequently, purification by column chromatography afforded the target compound 5-chloro-2,3-diphenyl-1H-indole (3ja) as a white solid in 90% yield.

References

[1] Chemical Communications, 2014, vol. 50, # 33, p. 4331 - 4334
[2] Patent: CN105218426, 2016, A. Location in patent: Paragraph 0039; 0040

5-CHLORO-2,3-DIPHENYL-1H-INDOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-CHLORO-2,3-DIPHENYL-1H-INDOLE Suppliers

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View Lastest Price from 5-CHLORO-2,3-DIPHENYL-1H-INDOLE manufacturers

Career Henan Chemical Co

Product: 5-CHLORO-2,3-DIPHENYL-1H-INDOLE 52598-02-4
Price: US $0.01/KG
Min. Order: 1KG
Purity: 98%; 99%
Supply Ability: 500g;1kg； 25kg
Release date: 2020-01-09

52598-02-4, 5-CHLORO-2,3-DIPHENYL-1H-INDOLERelated Search:

5-CHLORO-2,3-DIPHENYL-1H-INDOLE

1H-Indole, 5-chloro-2,3-diphenyl-

5-Chloro-2,3-diphenylindole

52598-02-4

C20H14ClN