Preparation
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HAFNIUM FLUORIDE

Preparation
Product Name
HAFNIUM FLUORIDE
CAS No.
13709-52-9
Chemical Name
HAFNIUM FLUORIDE
Synonyms
HAFNIUM FLUORIDE;HAFNIUM(IV) FLUORIDE;HAFNIUM TETRAFLUORIDE;Hafnium fluoride/ 99.9%;HAFNIUM FLUORIDE, 99.99%;Hafnium(IV) fluoride,98%;hafnium(4+):tetrafluoride;HAFNIUM TETRAFLUORIDE 99%;Hafnium tetrafluoride 99.9%;HafniuM(IV) fluoride, 98% 5GR
CBNumber
CB2756332
Molecular Formula
F4Hf
Formula Weight
254.48
MOL File
13709-52-9.mol
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HAFNIUM FLUORIDE Property

Melting point:
310°C (subl.)
Boiling point:
970°C
Density 
7.100
solubility 
reacts with H2O
form 
Powder
color 
White
Water Solubility 
React with water.
Sensitive 
Moisture Sensitive
Exposure limits
ACGIH: TWA 2.5 mg/m3; TWA 0.5 mg/m3
NIOSH: IDLH 250 mg/m3; IDLH 50 mg/m3; TWA 0.5 mg/m3
CAS DataBase Reference
13709-52-9(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi,T
Risk Statements 
32-36/37/38-41-23-37/38
Safety Statements 
26-36-45-36/37/39
RIDADR 
UN 2923 8/PG 2
WGK Germany 
3
Hazard Note 
Irritant
TSCA 
Yes
HazardClass 
6.1
PackingGroup 
II
HS Code 
28261990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H315Causes skin irritation

H318Causes serious eye damage

H331Toxic if inhaled

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
399868
Product name
Hafnium(IV) fluoride
Purity
99.9% trace metals basis (purity excludes up to ~1% zirconium)
Packaging
25g
Price
$352
Updated
2022/05/15
Alfa Aesar
Product number
036392
Product name
Hafnium(IV) fluoride, 99.9% (metals basis excluding Zr), Zr 2-4%
Packaging
5g
Price
$129
Updated
2021/12/16
Alfa Aesar
Product number
036392
Product name
Hafnium(IV) fluoride, 99.9% (metals basis excluding Zr), Zr 2-4%
Packaging
25g
Price
$428
Updated
2021/12/16
Alfa Aesar
Product number
045061
Product name
Hafnium(IV) fluoride, 99.9% (metals basis)
Packaging
25g
Price
$470
Updated
2023/06/20
Chem-Impex
Product number
35562
Product name
Hafnium(IV) fluoride
Purity
≥99.9% Metals basis excluding Zr (Zr : 2 - 4%)
Packaging
1G
Price
$35
Updated
2021/12/16
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HAFNIUM FLUORIDE Chemical Properties,Usage,Production

Preparation

Hafnium tetrafluoride may be prepared by passing anhydrous hydrogen fluoride over hafnium tetrachloride at 300°C:
HfCl4 + 4HF HfF4 + HCl
Another method of preparation involves thermal decomposition of ammonium fluorohafnate, (NH4)2 HfF6 [16925-24-9] in the absence of air:
(NH4)2 HfF6 HfF4 + 2NH3 + 2HF
Also, HfF4 can be prepared by treating metallic hafnium with 40% aqueous HF. The monohydrate formed may be heated at 350°C for several days under a flow of fluorine and nitrogen to yield anhydrous HfF4.
Hf + 4HF (aq) → HfF4•H2O + 2H2

Chemical Properties

Off-white powder

Physical properties

White monoclinic crystals; refractive index 1.56; density 7.1 g/cm3; sublimes at 970°C.

Uses

Hafnium(IV) fluoride is used as Vacuum deposition.

Production Methods

Hafnium tetrafluoride is prepared by careful thermal decomposition of ammonium fluorohafniate in an oxygen- free atmosphere or by passing anhydrous hydrogen fluoride over hafnium tetrachloride at 300℃. Direct synthesis from the elements is incomplete because the product merely forms a film on the metal. Ammonium fluorohafniate can be prepared by crystallization from an aqueous hydrofluoric acid solution by adding ammonium fluoride.

HAFNIUM FLUORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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HAFNIUM FLUORIDE Suppliers

Interchim S.A.
Tel
--
Fax
--
Email
interchim@interchim.com
Country
France
ProdList
6302
Advantage
76

13709-52-9, HAFNIUM FLUORIDERelated Search:


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