1-BOC-4-NITROINDOLE
- Product Name
- 1-BOC-4-NITROINDOLE
- CAS No.
- 913836-24-5
- Chemical Name
- 1-BOC-4-NITROINDOLE
- Synonyms
- 1-BOC-4-NITROINDOLE;N-BOC-4-NITROINDOLE;4-Nitroindole, N-BOC protected;4-Nitroindole,N-BOCprotected97%;4-Nitroindole, N-BOC protected 97%;TERT-BUTYL 4-NITRO-1H-INDOLE-1-CARBOXYLATE;4-nitro-1-indolecarboxylic acid tert-butyl ester;4-nitro-indole-1-carboxylic acid tert-butyl ester;1H-Indole-1-carboxylic acid, 4-nitro-, 1,1-dimethylethyl ester
- CBNumber
- CB2838773
- Molecular Formula
- C13H14N2O4
- Formula Weight
- 262.26
- MOL File
- 913836-24-5.mol
1-BOC-4-NITROINDOLE Property
- Melting point:
- 91-94
- Boiling point:
- 395.3±34.0 °C(Predicted)
- Density
- 1.26±0.1 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- Light yellow to yellow Solid
Safety
- Hazard Codes
- Xi
- Hazard Note
- Irritant
- HS Code
- 2933998090
N-Bromosuccinimide Price
- Product number
- B658105
- Product name
- 1-Boc-4-nitroindole
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- FB149267
- Product name
- 1-Boc-4-nitroindole
- Packaging
- 500mg
- Price
- $100
- Updated
- 2021/12/16
- Product number
- V9052
- Product name
- 1-BOC-4-nitroindole
- Packaging
- 1g
- Price
- $109
- Updated
- 2021/12/16
- Product number
- 4H54-1-0U
- Product name
- 4-Nitroindole, N-Boc protected
- Purity
- 97%
- Packaging
- 1g
- Price
- $112
- Updated
- 2021/12/16
- Product number
- FB149267
- Product name
- 1-Boc-4-nitroindole
- Packaging
- 250mg
- Price
- $57.5
- Updated
- 2021/12/16
1-BOC-4-NITROINDOLE Chemical Properties,Usage,Production
Synthesis
4769-97-5
24424-99-5
913836-24-5
A catalytic amount of 4-dimethylaminopyridine (DMAP) and di-tert-butyl dicarbonate (Boc2O, 5.9 g, 27.1 mmol) were sequentially added to a stirred solution of 4-nitroindole (4.0 g, 24.6 mmol) in dichloromethane (50 mL) at 0 °C. The reaction mixture was continued to be stirred at room temperature for 3 hours. After completion of the reaction, the reaction mixture was diluted with dichloromethane and washed with deionized water. The organic phase was separated and dried over anhydrous magnesium sulfate. The solvent was removed by concentration under reduced pressure to give 1-Boc-4-nitroindole as a white solid (6.14 g, 95% yield). Mass spectrum (ESI) m/z 262.1.
References
[1] Patent: US2009/227575, 2009, A1. Location in patent: Page/Page column 20
[2] Patent: US2010/36123, 2010, A1. Location in patent: Page/Page column 4; 5; 7; 8
1-BOC-4-NITROINDOLE Preparation Products And Raw materials
Raw materials
Preparation Products
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