3-CHLORO-6-BENZYLOXYPYRIDAZINE
- Product Name
- 3-CHLORO-6-BENZYLOXYPYRIDAZINE
- CAS No.
- 91063-19-3
- Chemical Name
- 3-CHLORO-6-BENZYLOXYPYRIDAZINE
- Synonyms
- 3-CHLORO-6-BENZYLOXYPYRIDAZINE;3-chloro-6-phenylmethoxypyridazine;Pyridazine, 3-chloro-6-(phenylmethoxy)-
- CBNumber
- CB2839255
- Molecular Formula
- C11H9ClN2O
- Formula Weight
- 220.65
- MOL File
- 91063-19-3.mol
3-CHLORO-6-BENZYLOXYPYRIDAZINE Property
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B704313
- Product name
- 3-(Benzyloxy)-6-chloropyridazine
- Packaging
- 100mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- FB142751
- Product name
- 3-(Benzyloxy)-6-chloropyridazine
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- FB142751
- Product name
- 3-(Benzyloxy)-6-chloropyridazine
- Packaging
- 1g
- Price
- $115
- Updated
- 2021/12/16
- Product number
- FB142751
- Product name
- 3-(Benzyloxy)-6-chloropyridazine
- Packaging
- 2g
- Price
- $200
- Updated
- 2021/12/16
- Product number
- 5198AC
- Product name
- 3-(Benzyloxy)-6-chloropyridazine
- Packaging
- 5g
- Price
- $253
- Updated
- 2021/12/16
3-CHLORO-6-BENZYLOXYPYRIDAZINE Chemical Properties,Usage,Production
Synthesis
141-30-0
20194-18-7
91063-19-3
Procedure for the synthesis of 3-(benzyloxy)-6-chloropyridazine: 33.92 g (205.5 mmol) of 3,6-dichloropyridazine was dissolved in 100 mL of benzyl alcohol, followed by the addition of 30.06 g (231.0 mmol) of sodium benzyl alcohol. The reaction mixture was stirred at room temperature for 30 minutes. Upon completion of the reaction, the mixture was slowly poured into ice water and the precipitate was collected by filtration and washed with distilled water. The resulting product was dried at 80 °C to give 11.5 g of the target compound in 81% yield of the theoretical value. The Rf value of the product was 0.60 (silica gel plate, unfolding agent was cyclohexane/ethyl acetate = 2:1). The molecular weight of the product was confirmed to be 243/245 [M+Na]+ by EII mass spectrometry.
References
[1] Patent: WO2007/48802, 2007, A1. Location in patent: Page/Page column 79
3-CHLORO-6-BENZYLOXYPYRIDAZINE Preparation Products And Raw materials
Raw materials
Preparation Products
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