5-Methyl-2-mercaptobenzothiazole
- Product Name
- 5-Methyl-2-mercaptobenzothiazole
- CAS No.
- 21303-50-4
- Chemical Name
- 5-Methyl-2-mercaptobenzothiazole
- Synonyms
- 5-Methyl-2-benzothiazolethiol;5-Methylbenzo[d]thiazole-2-thiol;2-Mercapto-5-methyl bezimidazole;2-Mercapto-5-methylbenzothiazole;5-Methyl-2-mercaptobenzothiazole;5-Methyl-2(3H)-benzothiazolethione;2(3H)-Benzothiazolethione, 5-methyl-;5-Methylbenzo[d]thiazole-2(3h)-thione;5-methyl-3H-1,3-benzothiazole-2-thione;2(3H)-Benzothiazolethione,5-methyl-(9CI)
- CBNumber
- CB2969192
- Molecular Formula
- C8H7NS2
- Formula Weight
- 181.28
- MOL File
- 21303-50-4.mol
5-Methyl-2-mercaptobenzothiazole Property
- Melting point:
- 121 °C
- Boiling point:
- 314 °C
- Density
- 1.39
- Flash point:
- 144 °C
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 9.60±0.20(Predicted)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H319Causes serious eye irritation
- Precautionary statements
-
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- AA0072W8
- Product name
- 5-Methylbenzo[d]thiazole-2-thiol
- Purity
- 98%
- Packaging
- 10g
- Price
- $1138
- Updated
- 2026/05/28
- Product number
- AD288517
- Product name
- 5-Methylbenzo[d]thiazole-2(3h)-thione
- Purity
- 95%
- Packaging
- 1G
- Price
- $230
- Updated
- 2026/05/27
- Product number
- AD288517
- Product name
- 5-Methylbenzo[d]thiazole-2(3h)-thione
- Purity
- 95%
- Packaging
- 5G
- Price
- $920
- Updated
- 2026/05/27
- Product number
- CD11166197
- Product name
- 5-Methylbenzo[d]thiazole-2-thiol
- Purity
- 95+%
- Packaging
- 1g
- Price
- $345
- Updated
- 2026/05/26
- Product number
- CM161504
- Product name
- 5-Methylbenzo[d]thiazole-2-thiol
- Purity
- 95%
- Packaging
- 1g
- Price
- $144
- Updated
- 2026/05/26
5-Methyl-2-mercaptobenzothiazole Chemical Properties,Usage,Production
Synthesis
75-15-0
95-81-8
21303-50-4
Synthesis of 5-methyl-2-mercaptobenzothiazole (10): 2-chloro-5-methylaniline (9, 1.00 g, 7.06 mmol) and potassium carbonate (K2CO3, 2.80 g, 28.2 mmol) were suspended in N,N-dimethylformamide (DMF, 20 mL) under protection of nitrogen. Subsequently, carbon disulfide (CS2, 0.50 mL, 8.50 mmol) was added to the suspension. The reaction mixture was heated and reacted at 150 °C for 16 hours. Upon completion of the reaction, it was cooled to room temperature, the reaction mixture was diluted with deionized water (30 mL) and acidified with 1 N hydrochloric acid (HCl) to a pH of about 1. The resulting precipitate was collected by filtration, washed several times with deionized water, and finally dried under vacuum in the presence of phosphorus pentoxide (P2O5) to afford the target product 5-methyl-2-mercaptobenzothiazole (10, 0.35 g, Yield 27%).
References
[1] Patent: WO2006/122156, 2006, A2. Location in patent: Page/Page column 126
5-Methyl-2-mercaptobenzothiazole Preparation Products And Raw materials
Raw materials
Preparation Products
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