ChemicalBook > CAS DataBase List > 4-(METHYLSULFONYLAMINO)BENZYLAMINEHYDROCHLORIDE

4-(METHYLSULFONYLAMINO)BENZYLAMINEHYDROCHLORIDE

Product Name
4-(METHYLSULFONYLAMINO)BENZYLAMINEHYDROCHLORIDE
CAS No.
128263-66-1
Chemical Name
4-(METHYLSULFONYLAMINO)BENZYLAMINEHYDROCHLORIDE
Synonyms
4-(Methylsulfonylamino)benzylamine, HCl;N-(4-(AMinoMethyl)phenyl)MethanesulfonaMide hydrochloride;N-[4-(Aminomethyl)phenyl]methanesulphonamide hydrochloride;N-[4-(Aminomethyl)phenyl]methanesulphonamide hydrochloride 95+%;Methanesulfonamide, N-[4-(aminomethyl)phenyl]-, hydrochloride (1:1);4-(Methylsulfonylamino)benzylamine hydrochloride(Methylsulfonylamino)Benzylaminehydrochloride;4-[(Methylsulphonyl)amino]benzylamine hydrochloride, 4-(Methylsulphonamido)benzylamine hydrochloride
CBNumber
CB31096535
Molecular Formula
C8H13ClN2O2S
Formula Weight
236.72
MOL File
128263-66-1.mol
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4-(METHYLSULFONYLAMINO)BENZYLAMINEHYDROCHLORIDE Property

Melting point:
>275℃ (dec.)
storage temp. 
Inert atmosphere,Room Temperature
form 
solid
color 
White
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Safety

HazardClass 
IRRITANT
HS Code 
2935909099
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
M219093
Product name
4-(Methylsulfonylamino)benzylamineHydrochloride
Packaging
50mg
Price
$60
Updated
2021/12/16
TRC
Product number
M219093
Product name
4-(Methylsulfonylamino)benzylamineHydrochloride
Packaging
250mg
Price
$90
Updated
2021/12/16
SynQuest Laboratories
Product number
8669-5-X5
Product name
N-[4-(Aminomethyl)phenyl]methanesulfonamide hydrochloride
Packaging
1g
Price
$125
Updated
2021/12/16
Matrix Scientific
Product number
012580
Product name
4-(Methylsulfonylamino)benzylamine hydrochloride
Purity
98%
Packaging
1g
Price
$134
Updated
2021/12/16
AK Scientific
Product number
5409AA
Product name
N-(4-(Aminomethyl)phenyl)methanesulfonamidehydrochloride
Packaging
1g
Price
$142
Updated
2021/12/16
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4-(METHYLSULFONYLAMINO)BENZYLAMINEHYDROCHLORIDE Chemical Properties,Usage,Production

Synthesis

238427-63-9

128263-66-1

Step 4: Synthesis of 4-methanesulfonylaminobenzylcarbamate hydrochloride; To a 50 mL single-necked round-bottomed flask was added tert-butyl 4-methanesulfonylaminobenzylcarbamate (1.2 g, 4.0 mmol) and 30 mL of 1,4-dioxane. Concentrated hydrochloric acid (2 mL) was slowly added to the solution and the reaction was stirred for 4 hours at room temperature. The progress of the reaction was monitored by thin layer chromatography (TLC) and after confirming the completion of the reaction, the reaction mixture was concentrated under reduced pressure to remove the solvent. The resulting solid was washed with ethyl acetate and separated by filtration through a glass filter. Finally, the collected solid was dried in air to afford the target product 4-methylsulfonylaminobenzylamine hydrochloride (0.947 g, 100% yield).

References

[1] Patent: WO2006/98554, 2006, A1. Location in patent: Page/Page column 44

4-(METHYLSULFONYLAMINO)BENZYLAMINEHYDROCHLORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-(METHYLSULFONYLAMINO)BENZYLAMINEHYDROCHLORIDE Suppliers

J & K SCIENTIFIC LTD.
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021 51613951
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China
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128263-66-1, 4-(METHYLSULFONYLAMINO)BENZYLAMINEHYDROCHLORIDE Related Search:


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  • 128263-66-1