ChemicalBook > CAS DataBase List > 5-CHLORO-1-METHYL-1H-INDOLE-2-CARBOXYLIC ACID

5-CHLORO-1-METHYL-1H-INDOLE-2-CARBOXYLIC ACID

Product Name: 5-CHLORO-1-METHYL-1H-INDOLE-2-CARBOXYLIC ACID
CAS No.: 59908-47-3
Chemical Name: 5-CHLORO-1-METHYL-1H-INDOLE-2-CARBOXYLIC ACID
Synonyms: AKOS JY2082728;TIMTEC-BB SBB011233;ASINEX-REAG BAS 10142185;5-chloro-1-methyl-2-indolecarboxylic acid;5-chloro-1-methylindole-2-carboxylic acid;5-CHLORO-1-METHYL-1H-INDOLE-2-CARBOXYLIC ACID;1H-Indole-2-carboxylic acid, 5-chloro-1-Methyl-;5,7-diethyl-2-(3-nitrophenyl)-1,3-diazaadamantan-8-one
CBNumber: CB3131970
Molecular Formula: C10H8ClNO2
Formula Weight: 209.63
MOL File: Mol file

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5-CHLORO-1-METHYL-1H-INDOLE-2-CARBOXYLIC ACID Property

Boiling point:: 420.6±25.0 °C(Predicted)
Density: 1.39±0.1 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 3.93±0.30(Predicted)
Appearance: White to light yellow Solid

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Safety

Hazard Codes: Xi,Xn
Risk Statements: 22
HazardClass: IRRITANT
HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P330Rinse mouth.

P363Wash contaminated clothing before reuse.

P403Store in a well-ventilated place.

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N-Bromosuccinimide Price

TRC

Product number: C994855
Product name: 5-Chloro-1-methyl-1H-indole-2-carboxylicAcid
Packaging: 10mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC118365
Product name: 5-Chloro-1-methyl-1H-indole-2-carboxylic acid
Packaging: 100mg
Price: $58
Updated: 2021/12/16

ChemScene

Product number: CS-W006501
Product name: 5-Chloro-1-methyl-1H-indole-2-carboxylicacid
Packaging: 250mg
Price: $63
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC118365
Product name: 5-Chloro-1-methyl-1H-indole-2-carboxylic acid
Packaging: 250mg
Price: $115
Updated: 2021/12/16

AK Scientific

Product number: 8930AB
Product name: 5-Chloro-1-methyl-1H-indole-2-carboxylicacid
Packaging: 250mg
Price: $145
Updated: 2021/12/16

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5-CHLORO-1-METHYL-1H-INDOLE-2-CARBOXYLIC ACID Chemical Properties,Usage,Production

Synthesis

148356-79-0

59908-47-3

Step 2: Synthesis of 5-chloro-1-methyl-1H-indole-2-carboxylic acid (43.2) To a THF solution (10 mL) of methyl 5-chloro-1-methyl-1H-indole-2-carboxylate (43.1, 224 mg) was added an aqueous solution (2 mL) of LiOH (36 mg, 1.5 mmol). The reaction mixture was stirred at room temperature for 2 hours. Upon completion of the reaction, the solvent was removed under reduced pressure and the residue was dissolved in 1N aqueous hydrochloric acid solution (10 mL). The resulting suspension was allowed to stand for 10 minutes, then filtered through filter paper, collected as a solid and dried under vacuum to afford 163 mg (77.6% yield) of 5-chloro-1-methyl-1H-indole-2-carboxylic acid (43.2) as a beige powder.

References

[1] Patent: KR101725451, 2017, B1. Location in patent: Paragraph 0294; 0301-0303
[2] Patent: WO2016/40449, 2016, A1. Location in patent: Paragraph 00508-00509
[3] Patent: WO2006/66879, 2006, A2. Location in patent: Page/Page column 53; 48
[4] Bioorganic and Medicinal Chemistry, 2018, vol. 26, # 21, p. 5664 - 5671

5-CHLORO-1-METHYL-1H-INDOLE-2-CARBOXYLIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-CHLORO-1-METHYL-1H-INDOLE-2-CARBOXYLIC ACID manufacturers

Career Henan Chemical Co

Product: 5-CHLORO-1-METHYL-1H-INDOLE-2-CARBOXYLIC ACID 59908-47-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: Customized
Release date: 2020-03-05

59908-47-3, 5-CHLORO-1-METHYL-1H-INDOLE-2-CARBOXYLIC ACIDRelated Search:

TIMTEC-BB SBB011233

AKOS JY2082728

5-CHLORO-1-METHYL-1H-INDOLE-2-CARBOXYLIC ACID

ASINEX-REAG BAS 10142185

1H-Indole-2-carboxylic acid, 5-chloro-1-Methyl-

5-chloro-1-methylindole-2-carboxylic acid

5-chloro-1-methyl-2-indolecarboxylic acid

5,7-diethyl-2-(3-nitrophenyl)-1,3-diazaadamantan-8-one

59908-47-3