ETHYL 2-IODOBENZOATE
- Product Name
- ETHYL 2-IODOBENZOATE
- CAS No.
- 1829-28-3
- Chemical Name
- ETHYL 2-IODOBENZOATE
- Synonyms
- RARECHEM AL BI 0562;ETHYL 2-IODOBENZOATE;ETHYL O-IODOBENZOATE;E**Ethyl 2-iodobenzoate;2-(Ethoxycarbonyl)iodobenzene
- CBNumber
- CB3141564
- Molecular Formula
- C9H9IO2
- Formula Weight
- 276.07
- MOL File
- 1829-28-3.mol
ETHYL 2-IODOBENZOATE Property
- Boiling point:
- 163-165°C/23mm
- Density
- 1.664±0.06 g/cm3(Predicted)
- refractive index
- 1.584
- Flash point:
- 163-165°C/23mm
- storage temp.
- 2-8°C(protect from light)
- solubility
- Difficult to mix.
- form
- clear liquid
- color
- Colorless to Light yellow to Light orange
- Sensitive
- Light Sensitive
- BRN
- 2084297
Safety
- Hazard Codes
- Xi
- HazardClass
- IRRITANT, LIGHT SENSITIVE
- HS Code
- 2916399090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- E1273
- Product name
- Ethyl 2-Iodobenzoate
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $28
- Updated
- 2025/07/31
- Product number
- E1273
- Product name
- Ethyl 2-Iodobenzoate
- Purity
- >98.0%(GC)
- Packaging
- 25g
- Price
- $79
- Updated
- 2025/07/31
- Product number
- B124713
- Product name
- Ethyl 2-Iodobenzoate
- Packaging
- 500mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- B124713
- Product name
- Ethyl 2-Iodobenzoate
- Packaging
- 2.5g
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 012667
- Product name
- Ethyl 2-iodobenzoate
- Purity
- 98%
- Packaging
- 5g
- Price
- $14
- Updated
- 2021/12/16
ETHYL 2-IODOBENZOATE Chemical Properties,Usage,Production
Uses
Ethyl 2-iodobenzoate is used as anti-infective, contraceptive agent and x-ray contrast medium for diagnostic radiology.
Synthesis
64-17-5
88-67-5
1829-28-3
General procedure for the synthesis of ethyl 2-iodobenzoate from ethanol and 2-iodobenzoic acid: 2-iodobenzoic acid (10 g) was dissolved in 60 mL of ethanol and 5 mL of concentrated H2SO4 was added as a catalyst. The reaction mixture was placed in an oil bath at 78 °C with electromagnetic stirring for 5 hours. Upon completion of the reaction, excess ethanol was removed under reduced pressure using a rotary evaporator. Water and ethyl acetate were added to the residue to separate the organic layer. The organic layer was washed three times sequentially with water and saturated sodium bicarbonate solution. Finally, the organic layer was dried with anhydrous Na2SO4, filtered and the solvent was removed by distillation to afford ethyl 2-iodobenzoate in 99% yield.
References
[1] Synthetic Communications, 2017, vol. 47, # 12, p. 1175 - 1184
[2] Bioorganic and Medicinal Chemistry Letters, 2006, vol. 16, # 18, p. 4822 - 4825
[3] Tetrahedron Letters, 2014, vol. 55, # 3, p. 690 - 693
[4] Patent: US2010/216853, 2010, A1. Location in patent: Page/Page column 19-20
[5] Tetrahedron Letters, 1996, vol. 37, # 35, p. 6375 - 6378
ETHYL 2-IODOBENZOATE Preparation Products And Raw materials
Raw materials
Preparation Products
ETHYL 2-IODOBENZOATE Suppliers
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View Lastest Price from ETHYL 2-IODOBENZOATE manufacturers
- Product
- ETHYL 2-IODOBENZOATE 1829-28-3
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-06-27