Benzene, 2-chloro-1-methoxy-3-nitro-
- Product Name
- Benzene, 2-chloro-1-methoxy-3-nitro-
- CAS No.
- 3970-39-6
- Chemical Name
- Benzene, 2-chloro-1-methoxy-3-nitro-
- Synonyms
- 2-Chloro-3-nitroanisole;2-chloro-1-Methoxy-3-nitro-;2-Chloro-1-methoxy-3-nitrobenzene;2-Chloro-3-methoxy-1-nitrobenzene;Benzene, 2-chloro-1-methoxy-3-nitro-;2-Chloro-1-methoxy-3-nitrobenzene, 95
- CBNumber
- CB31465661
- Molecular Formula
- C7H6ClNO3
- Formula Weight
- 187.58
- MOL File
- 3970-39-6.mol
Benzene, 2-chloro-1-methoxy-3-nitro- Property
- Melting point:
- 93-94 °C
- Boiling point:
- 290.3±20.0 °C(Predicted)
- Density
- 1.366±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- wooly powder
- color
- Gold to faint tan
Safety
- HS Code
- 2909309090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- C596515
- Product name
- 2-Chloro-1-methoxy-3-nitrobenzene
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- C596515
- Product name
- 2-Chloro-1-methoxy-3-nitrobenzene
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- FC144357
- Product name
- 2-Chloro-1-methoxy-3-nitrobenzene
- Packaging
- 1g
- Price
- $63
- Updated
- 2021/12/16
- Product number
- OR55654
- Product name
- 2-Chloro-1-methoxy-3-nitrobenzene
- Purity
- 97%
- Packaging
- 5g
- Price
- $63
- Updated
- 2021/12/16
- Product number
- FC144357
- Product name
- 2-Chloro-1-methoxy-3-nitrobenzene
- Packaging
- 10g
- Price
- $372
- Updated
- 2021/12/16
Benzene, 2-chloro-1-methoxy-3-nitro- Chemical Properties,Usage,Production
Synthesis
603-84-9
74-88-4
3970-39-6
Step B: 2-chloro-3-nitrophenol (1.3 g, 7.49 mmol) was dissolved in N,N-dimethylformamide (DMF, 10 ml), to which milled cesium carbonate (2.92 g, 8.96 mmol) was added, followed by dropwise addition of iodomethane (1.4 ml, 22.5 mmol). The reaction mixture was stirred at room temperature overnight. After completion of the reaction, DMF was removed by distillation under reduced pressure, the residue was dissolved in ether (150 ml), the organic phase was washed sequentially with water (150 ml) and saturated saline (4 x 100 ml) and then dried with anhydrous magnesium sulfate. After filtering to remove the drier, the organic phase was concentrated under reduced pressure to obtain the crude 2-chloro-3-nitroanisole (1.38 g, yield 98%) as an orange solid.
References
[1] Patent: WO2004/103996, 2004, A1. Location in patent: Page 42-43
[2] Patent: WO2006/7700, 2006, A1. Location in patent: Page/Page column 63
[3] Patent: US2006/19905, 2006, A1. Location in patent: Page/Page column 25
[4] Patent: WO2006/85, 2006, A1. Location in patent: Page/Page column 77
[5] Chemische Berichte, 1893, vol. 26, p. 2466
Benzene, 2-chloro-1-methoxy-3-nitro- Preparation Products And Raw materials
Raw materials
Preparation Products
Benzene, 2-chloro-1-methoxy-3-nitro- Suppliers
- Tel
- --
- Fax
- --
- info@fchgroup.net
- Country
- Ukraine
- ProdList
- 721
- Advantage
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View Lastest Price from Benzene, 2-chloro-1-methoxy-3-nitro- manufacturers
- Product
- Benzene, 2-chloro-1-methoxy-3-nitro- 3970-39-6
- Price
- US $6.60/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 1kg -1000kg
- Release date
- 2020-01-02