5-BROMO-2-ISOPROPOXYBENZALDEHYDE

Product Name: 5-BROMO-2-ISOPROPOXYBENZALDEHYDE
CAS No.: 138505-25-6
Chemical Name: 5-BROMO-2-ISOPROPOXYBENZALDEHYDE
Synonyms: 5-BROMO-2-ISOPROPOXYBENZALDEHYDE;5-bromo-2-propan-2-yloxybenzaldehyde;5-bromo-2-propan-2-yloxy-benzaldehyde;5-Bromo-2-(1-methylethoxy)benzaldehyde;Benzaldehyde, 5-bromo-2-(1-methylethoxy)-
CBNumber: CB31498999
Molecular Formula: C10H11BrO2
Formula Weight: 243.1
MOL File: 138505-25-6.mol

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5-BROMO-2-ISOPROPOXYBENZALDEHYDE Property

Melting point:: 31-33 °C
Boiling point:: 309.7±22.0 °C(Predicted)
Density: 1.391±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: Colorless to light yellow <31°C Solid,>33°C Oil

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: B686238
Product name: 5-Bromo-2-isopropoxybenzaldehyde
Packaging: 500mg
Price: $155
Updated: 2021/12/16

Matrix Scientific

Product number: 028567
Product name: 5-Bromo-2-isopropoxybenzaldehyde
Packaging: 1g
Price: $168
Updated: 2021/12/16

AK Scientific

Product number: 4081AD
Product name: 5-Bromo-2-isopropoxybenzaldehyde
Packaging: 1g
Price: $203
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB113055
Product name: 5-Bromo-2-isopropoxybenzaldehyde
Packaging: 2g
Price: $289
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB113055
Product name: 5-Bromo-2-isopropoxybenzaldehyde
Packaging: 500mg
Price: $100
Updated: 2021/12/16

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5-BROMO-2-ISOPROPOXYBENZALDEHYDE Chemical Properties,Usage,Production

Synthesis

75-30-9

1761-61-1

138505-25-6

Step A: Synthesis of 5-bromo-2-isopropoxybenzaldehyde (AX). To a suspension of dimethylformamide (DMF) containing potassium carbonate (34.4 g, 249 mmol) and cesium carbonate (16.2 g, 50 mmol) were sequentially added 5-bromosalicylaldehyde (25.0 g, 124 mmol) and 2-iodopropane (25.0 mL, 249 mmol). The reaction mixture was stirred at room temperature overnight, followed by heating to 70 °C and continued stirring for 4 hours. Upon completion of the reaction, the volatile solvent was removed by rotary evaporation. The residue was dissolved and partitioned between methyl tertiary butyl ether (MTBE) and water. The aqueous layer was further extracted with MTBE and all organic phases were combined and washed sequentially with water, sodium hydroxide solution and saturated brine. The organic layer was dried over anhydrous magnesium sulfate and concentrated to dryness under reduced pressure to afford 5-bromo-2-isopropoxybenzaldehyde (AX, 30.0 g) as a light yellow oil in 99% yield.1H NMR (CDCl3, 400 MHz): δ 1.40 (d, J = 6.3 Hz, 6H), 4.65 (sept, J = 6.0 Hz, 1H), 6.89 (d, J = 9.0 Hz, 1H), 7.59 (dd, J = 9.0 and 2.7 Hz, 1H), 7.91 (d, J = 2.7 Hz, 1H), 10.39 (s, 1H).

References

[1] Patent: US2009/202480, 2009, A1
[2] Tetrahedron Letters, 2010, vol. 51, # 4, p. 709 - 713
[3] Patent: US9115095, 2015, B2. Location in patent: Page/Page column 44; 45
[4] Synlett, 2016, vol. 27, # 16, p. 2352 - 2356
[5] Helvetica Chimica Acta, 2005, vol. 88, # 5, p. 936 - 949

5-BROMO-2-ISOPROPOXYBENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-BROMO-2-ISOPROPOXYBENZALDEHYDE manufacturers

Hefei Lbao Physical & Chemical Science Co.,Ltd

Product: 5-Bromo-2-isopropoxybenzaldehyde 138505-25-6
Price: US $0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: Customise
Release date: 2025-10-24

138505-25-6, 5-BROMO-2-ISOPROPOXYBENZALDEHYDERelated Search:

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5-BROMO-2-ISOPROPOXYBENZALDEHYDE

5-Bromo-2-(1-methylethoxy)benzaldehyde

5-bromo-2-propan-2-yloxybenzaldehyde

5-bromo-2-propan-2-yloxy-benzaldehyde

Benzaldehyde, 5-bromo-2-(1-methylethoxy)-

138505-25-6