2(1H)-PYRIDINONE, 1-METHYL-5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-

Uses

Product Name: 2(1H)-PYRIDINONE, 1-METHYL-5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-
CAS No.: 1002309-52-5
Chemical Name: 2(1H)-PYRIDINONE, 1-METHYL-5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-
Synonyms: 1-Methyl-5-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)pyridin-2(1H)-one;1-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-one;N-Methyl-1H-pyridin-2-one-5-boronic acid, pinacol ester;1-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyri...;1-Methyl-6-oxo-1,6-dihydropyridine-3-boronic Acid Pinacol Ester;1-methyl-6-oxo-1,6-dihydropyridin-3-ylboronic acid pinacol ester;1-METHYL-5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-2(1H)-PYRIDINONE;1-Methyl-5-(tetraMethyl-1,3,2-dioxaborolan-2-yl)-1,2-dihydropyridin-2-one;1-METHYL-5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-1H-PYRIDIN-2-ONE;2(1H)-PYRIDINONE, 1-METHYL-5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-
CBNumber: CB31502641
Molecular Formula: C12H18BNO3
Formula Weight: 235.09
MOL File: 1002309-52-5.mol

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2(1H)-PYRIDINONE, 1-METHYL-5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)- Property

Boiling point:: 287.1±50.0 °C(Predicted)
Density: 1.09±0.1 g/cm3(Predicted)
storage temp.: Inert atmosphere,Store in freezer, under -20°C
pka: 0.03±0.62(Predicted)
form: solid
color: Beige
InChI: InChI=1S/C12H18BNO3/c1-11(2)12(3,4)17-13(16-11)9-6-7-10(15)14(5)8-9/h6-8H,1-5H3
InChIKey: IJUNZKOKAXJGRQ-UHFFFAOYSA-N
SMILES: C1(=O)N(C)C=C(B2OC(C)(C)C(C)(C)O2)C=C1

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

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N-Bromosuccinimide Price

TRC

Product number: M338038
Product name: 1-Methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2(1H)-one
Packaging: 50mg
Price: $45
Updated: 2021/12/16

TRC

Product number: M338038
Product name: 1-Methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2(1H)-one
Packaging: 100mg
Price: $60
Updated: 2021/12/16

ChemScene

Product number: CS-W004791
Product name: 1-Methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2(1H)-one
Purity: >98.0%
Packaging: 1g
Price: $67
Updated: 2021/12/16

Apolloscientific

Product number: OR46124
Product name: 1-Methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2(1H)-one
Purity: 98%
Packaging: 1g
Price: $182
Updated: 2021/12/16

SynQuest Laboratories

Product number: 6H60-1-1W
Product name: 1-Methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2(1H)-one
Packaging: 1g
Price: $200
Updated: 2021/12/16

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2(1H)-PYRIDINONE, 1-METHYL-5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)- Chemical Properties,Usage,Production

Uses

1-Methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2(1H)-one is a useful research chemical.

Synthesis

81971-39-3

73183-34-3

1002309-52-5

A dioxane (5 mL) solution of potassium acetate (270 mg, 2.67 mmol) and Pd(dppf)Cl2 (80 mg, 0.11 mmol) was added as 5-bromo-1-methylpyridin-2-one (200.0 mg, 1.06 mmol) and bis(pinacolato)diboron (410.0 mg, 1.61 mmol). The reaction mixture was microwaved at 100 °C for 2 hours. After completion of the reaction, the mixture was filtered, washed with water and extracted with ethyl acetate (20 mL x 3). The organic phases were combined, dried with anhydrous sodium sulfate, filtered and concentrated to give the crude product 1-methyl-6-oxo-1,6-dihydropyridine-3-boronic acid pinacol ester (59.0 mg, 23.6% yield). The product was detected by LCMS and the molecular ion peak (M + H)+ was 236.

References

[1] Patent: US2015/111885, 2015, A1. Location in patent: Paragraph 0574; 0575
[2] Patent: EP2168965, 2010, A1. Location in patent: Page/Page column 33
[3] Patent: WO2008/8539, 2008, A2. Location in patent: Page/Page column 117-118
[4] Patent: WO2012/3189, 2012, A1. Location in patent: Page/Page column 81
[5] Patent: WO2011/60235, 2011, A1. Location in patent: Page/Page column 22

2(1H)-PYRIDINONE, 1-METHYL-5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)- Preparation Products And Raw materials

Raw materials

Preparation Products

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2(1H)-PYRIDINONE, 1-METHYL-5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)- Suppliers

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View Lastest Price from 2(1H)-PYRIDINONE, 1-METHYL-5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)- manufacturers

Career Henan Chemical Co

Product: 2(1H)-PYRIDINONE, 1-METHYL-5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)- 1002309-52-5
Price: US $5.50/KG
Min. Order: 1KG
Purity: 98%-99%
Supply Ability: 1kg-100kg
Release date: 2020-01-07

1002309-52-5, 2(1H)-PYRIDINONE, 1-METHYL-5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-Related Search:

2(1H)-PYRIDINONE, 1-METHYL-5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)- CIS-2-(2-BUTEN-1-YL)-4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLANE Allylboronic acid pinacol ester

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1-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyri...

1-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,2-dihydropyridin-2-one

1-Methyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-1H-pyridin-2-one - [M10345]

1002309-52-5