3-BENZYLOXYCARBONYLAMINO-CYCLOHEXANOL
- Product Name
- 3-BENZYLOXYCARBONYLAMINO-CYCLOHEXANOL
- CAS No.
- 955406-36-7
- Chemical Name
- 3-BENZYLOXYCARBONYLAMINO-CYCLOHEXANOL
- Synonyms
- Benzyl (3-hydroxycyclohexyl);3-BENZYLOXYCARBONYLAMINO-CYCLOHEXANOL;Benzyl (3-hydroxycyclohexyl)carbamate;(3-hydroxy-cyclohexyl)-carbamic acid benzyl ester;Carbamic acid,N-(3-hydroxycyclohexyl)-, phenylmethyl ester
- CBNumber
- CB31511647
- Molecular Formula
- C14H19NO3
- Formula Weight
- 249.31
- MOL File
- 955406-36-7.mol
3-BENZYLOXYCARBONYLAMINO-CYCLOHEXANOL Property
- Boiling point:
- 427.6±44.0 °C(Predicted)
- Density
- 1.17±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 12.11±0.40(Predicted)
- Appearance
- White to off-white Solid
N-Bromosuccinimide Price
- Product number
- 5224AQ
- Product name
- benzylN-(3-hydroxycyclohexyl)carbamate
- Packaging
- 250mg
- Price
- $161.6
- Updated
- 2021/12/16
- Product number
- CHM0378836
- Product name
- 3-N-CBZ-AMINOCYCLOHEXANOL
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $497.78
- Updated
- 2021/12/16
- Product number
- CS-0037998
- Product name
- Benzyl(3-hydroxycyclohexyl)carbamate
- Packaging
- 5g
- Price
- $874
- Updated
- 2021/12/16
- Product number
- 955406367
- Product name
- Benzyl(3-hydroxycyclohexyl)carbamate
- Packaging
- 5g
- Price
- $498.96
- Updated
- 2021/12/16
- Product number
- CD12001932
- Product name
- Benzyl(3-hydroxycyclohexyl)carbamate
- Purity
- 95+%
- Packaging
- 5g
- Price
- $499
- Updated
- 2021/12/16
3-BENZYLOXYCARBONYLAMINO-CYCLOHEXANOL Chemical Properties,Usage,Production
Synthesis
6850-39-1
501-53-1
955406-36-7
General procedure for the synthesis of benzyl (3-hydroxycyclohexyl) carbamate from 3-aminocyclohexanol and benzyl chloroformate: 3-hydroxycyclohexylamine (10 g, 86.96 mmol), potassium carbonate (18 g, 130 mmol), ethyl acetate (150 mL), and water (70 mL) were mixed, followed by the addition of benzyl chloroformate (22.17 g, 130 mmol). The reaction mixture was stirred at room temperature for 12 hours. Upon completion of the reaction, the organic layer was separated, dried over anhydrous sodium sulfate, filtered and concentrated. To the concentrated residue diethyl ether was added, a white precipitate was precipitated, filtered and air-dried to give benzyl (3-hydroxycyclohexyl) carbamate 19.1 g in 88% yield. Mass spectrum (m/z): 250 (M+).
References
[1] Patent: US2009/111800, 2009, A1. Location in patent: Page/Page column 40
[2] Patent: WO2014/145512, 2014, A2. Location in patent: Page/Page column 136; 137
3-BENZYLOXYCARBONYLAMINO-CYCLOHEXANOL Preparation Products And Raw materials
Raw materials
Preparation Products
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