ChemicalBook > CAS DataBase List > RARECHEM AL BF 0500

RARECHEM AL BF 0500

Product Name
RARECHEM AL BF 0500
CAS No.
87808-48-8
Chemical Name
RARECHEM AL BF 0500
Synonyms
RARECHEM AL BF 0500;Methyl 3-fluoro-4-methybenzoate;METHYL 3-FLUORO-4-METHYLBENZOATE;Methyl 3-fluoro-4-methylbenzoate, 98%;3-Fluoro-4-methyl-Benzoic acid methyl ester;Benzoic acid, 3-fluoro-4-methyl-, methyl ester
CBNumber
CB3224977
Molecular Formula
C9H9FO2
Formula Weight
168.16
MOL File
87808-48-8.mol
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RARECHEM AL BF 0500 Property

Boiling point:
222.1±28.0 °C(Predicted)
Density 
1.137±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
Appearance
Colorless to off-white Solid-liquid mixture
InChI
InChI=1S/C9H9FO2/c1-6-3-4-7(5-8(6)10)9(11)12-2/h3-5H,1-2H3
InChIKey
RAFFOVQBMRBRCS-UHFFFAOYSA-N
SMILES
C(OC)(=O)C1=CC=C(C)C(F)=C1
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Safety

HS Code 
2916399090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC
Product number
M305463
Product name
Methyl3-fluoro-4-methylbenzoate
Packaging
100mg
Price
$45
Updated
2021/12/16
TRC
Product number
M305463
Product name
Methyl3-fluoro-4-methylbenzoate
Packaging
500mg
Price
$65
Updated
2021/12/16
TRC
Product number
M305463
Product name
Methyl3-fluoro-4-methylbenzoate
Packaging
1g
Price
$75
Updated
2021/12/16
AK Scientific
Product number
W9017
Product name
Methyl3-fluoro-4-methylbenzoate
Packaging
5g
Price
$54
Updated
2021/12/16
AK Scientific
Product number
J51187
Product name
Methyl3-fluoro-4-methylbenzoate
Packaging
1g
Price
$20
Updated
2021/12/16
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RARECHEM AL BF 0500 Chemical Properties,Usage,Production

Synthesis

67-56-1

350-28-7

87808-48-8

Step 1: Synthesis of methyl 3-fluoro-4-methylbenzoate: 3-fluoro-4-methylbenzoic acid (20 g, 130 mmol) was dissolved in thionyl chloride (80 ml) and heated to reflux for 2 hrs (the reaction was monitored by TLC until the feedstock completely disappeared). Subsequently, excess thionyl chloride was removed by distillation under reduced pressure. The residue was cooled to 0 °C and methanol (100 ml) was slowly added dropwise under stirring. After the dropwise addition, the reaction mixture was continued to be stirred at room temperature for 1 hour. After completion of the reaction, the reaction mixture was concentrated under reduced pressure, diluted with ethyl acetate and washed with saturated saline. The organic layer was dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give methyl 3-fluoro-4-methylbenzoate as a white solid, which could be used directly in the subsequent reaction without further purification (Yield: 21 g, Yield: 96%).

References

[1] Organic Process Research and Development, 2008, vol. 12, # 6, p. 1137 - 1141
[2] Patent: WO2011/100433, 2011, A1. Location in patent: Page/Page column 56
[3] Patent: WO2014/102376, 2014, A1. Location in patent: Page/Page column 44-45
[4] Patent: WO2014/102377, 2014, A1. Location in patent: Page/Page column 49
[5] Patent: WO2012/80221, 2012, A1. Location in patent: Page/Page column 82

RARECHEM AL BF 0500 Preparation Products And Raw materials

Raw materials

Preparation Products

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RARECHEM AL BF 0500 Suppliers

China 77 Germany 1 India 2 United States 6 Global 86
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View Lastest Price from RARECHEM AL BF 0500 manufacturers

Career Henan Chemical Co
Product
RARECHEM AL BF 0500 87808-48-8
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
1000KGS
Release date
2019-12-18

87808-48-8, RARECHEM AL BF 0500Related Search:

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  • RARECHEM AL BF 0500
  • METHYL 3-FLUORO-4-METHYLBENZOATE
  • 3-Fluoro-4-methyl-Benzoic acid methyl ester
  • Benzoic acid, 3-fluoro-4-methyl-, methyl ester
  • Methyl 3-fluoro-4-methybenzoate
  • Methyl 3-fluoro-4-methylbenzoate, 98%
  • 87808-48-8
  • 87080-48-8