ETHYL 5-PHENYL-3-ISOXAZOLECARBOXYLATE

Product Name: ETHYL 5-PHENYL-3-ISOXAZOLECARBOXYLATE
CAS No.: 13599-24-1
Chemical Name: ETHYL 5-PHENYL-3-ISOXAZOLECARBOXYLATE
Synonyms: TIMTEC-BB SBB014614;ethyl 3-phenyl-5-isoxazolecarboxylate
CBNumber: CB32446692
Molecular Formula: C12H11NO3
Formula Weight: 217.22
MOL File: 13599-24-1.mol

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ETHYL 5-PHENYL-3-ISOXAZOLECARBOXYLATE Property

Melting point:: 47 °C
Boiling point:: 379.8±30.0 °C(Predicted)
Density: 1.173±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: -4.43±0.50(Predicted)
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: E926728
Product name: Ethyl3-Phenylisoxazole-5-carboxylate
Packaging: 1g
Price: $330
Updated: 2021/12/16

AK Scientific

Product number: 6412AA
Product name: Ethyl3-phenylisoxazole-5-carboxylate
Packaging: 1g
Price: $226
Updated: 2021/12/16

Matrix Scientific

Product number: 040787
Product name: Ethyl 3-phenylisoxazole-5-carboxylate
Packaging: 1g
Price: $250
Updated: 2021/12/16

Matrix Scientific

Product number: 040787
Product name: Ethyl 3-phenylisoxazole-5-carboxylate
Packaging: 5g
Price: $750
Updated: 2021/12/16

Ambeed

Product number: A171415
Product name: Ethyl3-phenylisoxazole-5-carboxylate
Purity: 97%
Packaging: 10g
Price: $373
Updated: 2021/12/16

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ETHYL 5-PHENYL-3-ISOXAZOLECARBOXYLATE Chemical Properties,Usage,Production

Synthesis

81745-44-0

623-47-2

13599-24-1

General procedure for the synthesis of ethyl 3-phenylisoxazole-5-carboxylate from (E)-N-hydroxybenzimidoyl chloride and ethyl propargylate: preparation of the intermediate 54-ethyl S-phenylisoxazole-δ-carboxylic acid ethyl ester. The reaction was carried out by stirring ethyl propiolate (0.657 mL, 6.43 mmol), (E)-N-hydroxybenzenecarboximidoyl chloride (0.500 g, 3.21 mmol), and sodium bicarbonate (0.818 g, 9.64 mmol) in a mixed solvent of ethyl acetate (16 mL) and water (1 mL) at room temperature overnight. After completion of the reaction, the reaction mixture was filtered and the filtrate was concentrated under reduced pressure. The crude product was purified by fast column chromatography on silica gel, the eluent being a heptane solution of 5% to 80% dichloromethane, to give 0.295 g of ethyl 3-phenylisoxazole-5-carboxylate in 42% yield.ESI/APCI (+): 218 (M + H).

References

[1] Patent: WO2010/142801, 2010, A1. Location in patent: Page/Page column 162-163

ETHYL 5-PHENYL-3-ISOXAZOLECARBOXYLATE Preparation Products And Raw materials

Raw materials

Preparation Products

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ETHYL 5-PHENYL-3-ISOXAZOLECARBOXYLATE Suppliers

China 21 India 1 United States 4 Global 26

SynAsst Chemical.

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View Lastest Price from ETHYL 5-PHENYL-3-ISOXAZOLECARBOXYLATE manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: 3-Phenylisoxazole-5-carboxylic acid 13599-24-1
Price: US $2.20-8.80/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 100kg
Release date: 2025-06-17

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: ETHYL 3-PHENYLISOXAZOLE-5-CARBOXYLATE 13599-24-1
Price: US $2.20-8.80/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 100kg
Release date: 2025-06-17

13599-24-1, ETHYL 5-PHENYL-3-ISOXAZOLECARBOXYLATERelated Search:

ETHYL 5-(4-CHLOROPHENYL)ISOXAZOLE-3-CARBOXYLATE ETHYL 5-(2,4-DICHLORO-5-FLUOROPHENYL)ISOXAZOLE-3-CARBOXYLATE ETHYL-5(3-FLUOROPHENYL)-ISOXAZOLE-3-CARBOXYLATE ETHYL 5-P-TOLYLISOXAZOLE-3-CARBOXYLATE ETHYL 5-(3-NITROPHENYL)-3-ISOXAZOLECARBOXYLATE ETHYL 5-(4-BROMOPHENYL)ISOXAZOLE-3-CARBOXYLATE ETHYL 5-(2,4-DICHLOROPHENYL)ISOXAZOLE-3-CARBOXYLATE ETHYL 5-(4-METHOXYPHENYL)ISOXAZOLE-3-CARBOXYLATE ETHYL 5-(4-(METHYLTHIO)PHENYL)ISOXAZOLE-3-CARBOXYLATE ETHYL 5-(4-FLUOROPHENYL)ISOXAZOLE-3-CARBOXYLATE 3-(4-NITRO-PHENYL)-ISOXAZOLE-5-CARBOXYLIC ACID ETHYL ESTER ETHYL 5-PHENYL-3-ISOXAZOLECARBOXYLATE

TIMTEC-BB SBB014614

ethyl 3-phenyl-5-isoxazolecarboxylate

13599-24-1