2-BROMO-6-(BROMOMETHYL)NAPHTHALENE
- Product Name
- 2-BROMO-6-(BROMOMETHYL)NAPHTHALENE
- CAS No.
- 305798-02-1
- Chemical Name
- 2-BROMO-6-(BROMOMETHYL)NAPHTHALENE
- Synonyms
- 2-BROMO-6-(BROMOMETHYL)NAPHTHALENE;NAPHTHALENE, 2-BROMO-6-(BROMOMETHYL)-
- CBNumber
- CB32451690
- Molecular Formula
- C11H8Br2
- Formula Weight
- 299.99
- MOL File
- 305798-02-1.mol
2-BROMO-6-(BROMOMETHYL)NAPHTHALENE Property
- Melting point:
- 124-125 °C
- Boiling point:
- 363.3±17.0 °C(Predicted)
- Density
- 1.772±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- Off-white to light yellow Solid
N-Bromosuccinimide Price
- Product number
- 3219AB
- Product name
- 2-Bromo-6-(bromomethyl)naphthalene
- Packaging
- 100mg
- Price
- $77
- Updated
- 2021/12/16
- Product number
- 098861
- Product name
- 2-Bromo-6-(bromomethyl)naphthalene
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $364
- Updated
- 2021/12/16
- Product number
- HCH0103793
- Product name
- 2-BROMO-6-(BROMOMETHYL)NAPHTHALENE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $497.83
- Updated
- 2021/12/16
- Product number
- 098861
- Product name
- 2-Bromo-6-(bromomethyl)naphthalene
- Purity
- 95+%
- Packaging
- 1g
- Price
- $807
- Updated
- 2021/12/16
- Product number
- 3219AB
- Product name
- 2-Bromo-6-(bromomethyl)naphthalene
- Packaging
- 10g
- Price
- $1242
- Updated
- 2021/12/16
2-BROMO-6-(BROMOMETHYL)NAPHTHALENE Chemical Properties,Usage,Production
Synthesis
100751-63-1
305798-02-1
General procedure for the synthesis of 2-bromo-6-(bromomethyl)naphthalene from 6-bromo-2-(hydroxymethyl)naphthalene: To a solution of (6-bromonaphthalen-2-yl)methanol (1.19 g, 5 mmol) in anhydrous ethyl ether (40 mL) was added phosphorus tribromide (PBr3, 1.52 g, 22 mmol) dropwise at 0 °C. The reaction mixture was stirred at room temperature for 3 hours. After the reaction was completed, the reaction mixture was neutralized with aqueous sodium bicarbonate (NaHCO3). The product was extracted with ether (40 mL x 2), the organic layers were combined and dried with anhydrous sodium sulfate (Na2SO4). After filtration, the organic phase was concentrated to obtain the crude product. Finally, the crude product was purified by fast silica gel column chromatography (eluent: petroleum ether) to afford the target compound 2-bromo-6-(bromomethyl)naphthalene (1d, 1.27 g, 85% yield) as a white solid.
References
[1] Patent: US2006/159953, 2006, A1. Location in patent: Page/Page column 4
[2] Journal of Organometallic Chemistry, 2013, vol. 745-746, p. 177 - 185
2-BROMO-6-(BROMOMETHYL)NAPHTHALENE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-BROMO-6-(BROMOMETHYL)NAPHTHALENE manufacturers
- Product
- 2-BROMO-6-(BROMOMETHYL)NAPHTHALENE 305798-02-1
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%HPLC
- Supply Ability
- 10t
- Release date
- 2019-12-24