ChemicalBook > CAS DataBase List > BIS(4-METHOXYBENZYL)AMINE HCL SALT

BIS(4-METHOXYBENZYL)AMINE HCL SALT

Product Name: BIS(4-METHOXYBENZYL)AMINE HCL SALT
CAS No.: 854391-95-0
Chemical Name: BIS(4-METHOXYBENZYL)AMINE HCL SALT
Synonyms: BIS(4-METHOXYBENZYL)AMINE HCL SALT;Bis(4-Methoxybenzyl)aMine hydrochloride
CBNumber: CB32457076
Molecular Formula: C16H19NO2.ClH
Formula Weight: 293.792
MOL File: 854391-95-0.mol

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BIS(4-METHOXYBENZYL)AMINE HCL SALT Property

Melting point:: 243-245 °C
storage temp.: Inert atmosphere,Room Temperature
Appearance: White to off-white Solid
InChI: InChI=1S/C16H19NO2.ClH/c1-18-15-7-3-13(4-8-15)11-17-12-14-5-9-16(19-2)10-6-14;/h3-10,17H,11-12H2,1-2H3;1H
InChIKey: BZIDDCTZNYMKMG-UHFFFAOYSA-N
SMILES: N(CC1=CC=C(OC)C=C1)CC1C=CC(OC)=CC=1.Cl

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC

Product number: M265828
Product name: Bis(4-methoxybenzyl)aminehydrochloride
Packaging: 50mg
Price: $60
Updated: 2021/12/16

AK Scientific

Product number: 4532CX
Product name: Bis(4-methoxybenzyl)aminehydrochloride
Packaging: 250mg
Price: $72
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0376670
Product name: BIS-(4-METHOXYBENZYL)AMINE HYDROCHLORIDE
Purity: 95.00%
Packaging: 5MG
Price: $495.17
Updated: 2021/12/16

Crysdot

Product number: CD12023929
Product name: Bis(4-methoxybenzyl)aminehydrochloride
Purity: 97%
Packaging: 100g
Price: $535
Updated: 2021/12/16

Alichem

Product number: 854391950
Product name: Bis(4-methoxybenzyl)aminehydrochloride
Packaging: 100g
Price: $540
Updated: 2021/12/16

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BIS(4-METHOXYBENZYL)AMINE HCL SALT Chemical Properties,Usage,Production

Synthesis

123-11-5

2393-23-9

854391-95-0

Preparation of Intermediate 1-16: p-Methoxybenzaldehyde (1.8 mL, 14.8 mmol) was mixed with 4-methoxybenzylamine (1.9 mL, 14.8 mmol) in 50 mL of ethanol and the reaction was carried out at reflux for 4 hours. Upon completion of the reaction, the mixture was cooled to 0 °C and sodium borohydride (562 mg, 14.8 mmol) was slowly added followed by stirring at room temperature for 18 hours. After cooling to 0 °C again, 50 mL of water and 250 mL of dichloromethane were added to separate the organic phase. The aqueous layer was further extracted with dichloromethane (2 x 250 mL). All organic layers were combined, dried with anhydrous magnesium sulfate, filtered and concentrated. The residue was dissolved in 100 mL of ether, cooled to 0 °C, and about 10 mL of a dioxane solution of 4N HCl was added slowly and stirred at 0 °C for 2 hours. The resulting white solid was collected by filtration and washed with ether/ethyl acetate to afford the target product bis-(4-methoxybenzyl)-amine hydrochloride (3.99 g, 91% yield). The product was characterized by 1H NMR (300 MHz, DMSO): δ 9.40 (s, 2H), 7.45 (d, J=8.7 Hz, 4H), 6.98 (d, J=8.7 Hz, 4H), 4.03 (s, 4H), 3.77 (s, 6H).

References

[1] Patent: WO2011/141713, 2011, A1. Location in patent: Page/Page column 88
[2] Patent: US2013/131057, 2013, A1. Location in patent: Paragraph 0278; 0279; 0280

BIS(4-METHOXYBENZYL)AMINE HCL SALT Preparation Products And Raw materials

Raw materials

Preparation Products

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854391-95-0, BIS(4-METHOXYBENZYL)AMINE HCL SALTRelated Search:

bis(p-methoxyphenyl)iodonium bromide BIS(4-METHOXYPHENYL)PHENYLPHOSPHINE BIS-(4-METHOXY-BENZYL)-AMINE 4,4'-DIMETHOXYDIPHENYLAMINE 4,4'-DIMETHOXYBENZHYDRYLAMINE 4,4-DIMETHOXYDIPHENYLMETHANE BIS(4-METHOXYPHENYL) DISULPHIDE Bis(4-methoxyphenyl)phosphine oxide TRIMETHOBENZAMIDE HYDROCHLORIDE Itopride hydrochloride ESCHSCHOLTZINE HCL BIS(4-METHOXYBENZYL)AMINE HCL SALT CALIFORNIDINE PERCHLORATE PAVINE HCL 3-(3-CHLORO-4-METHOXYBENZYL)-6,7-DIMETHOXY-2-[(2-METHYLBENZYL)SULFANYL]-4(3H)-QUINAZOLINIMINE 2-(BENZYLSULFANYL)-3-(3-CHLORO-4-METHOXYBENZYL)-6,7-DIMETHOXY-4(3H)-QUINAZOLINIMINE 3-(3-CHLORO-4-METHOXYBENZYL)-4-IMINO-6,7-DIMETHOXY-3,4-DIHYDRO-2(1H)-QUINAZOLINETHIONE BENZO[1,3]DIOXOL-5-YLMETHYL-(3-ETHOXY-4-METHOXY-BENZYL)-AMINE HYDROCHLORIDE

BIS(4-METHOXYBENZYL)AMINE HCL SALT

Bis(4-Methoxybenzyl)aMine hydrochloride

854391-95-0