ChemicalBook > CAS DataBase List > 3,6-DIIODO-9-PHENYL-9H-CARBAZOLE

3,6-DIIODO-9-PHENYL-9H-CARBAZOLE

Product Name: 3,6-DIIODO-9-PHENYL-9H-CARBAZOLE
CAS No.: 57103-21-6
Chemical Name: 3,6-DIIODO-9-PHENYL-9H-CARBAZOLE
Synonyms: 3,6-Diiodo-9-phenylcarbazole;3,6-Diiodo-9-phenylcarbazole>9H-Carbazole,3,6-diiodo-9-phenyl;3,6-DIIODO-9-PHENYL-9H-CARBAZOLE
CBNumber: CB32457258
Molecular Formula: C18H11I2N
Formula Weight: 495.1
MOL File: 57103-21-6.mol

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3,6-DIIODO-9-PHENYL-9H-CARBAZOLE Property

Melting point:: 181.0 to 185.0 °C
Boiling point:: 540.8±43.0 °C(Predicted)
Density: 1.94±0.1 g/cm3(Temp: 20 °C; Press: 760 Torr)(Predicted)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
solubility: slightly sol. in dichloromethane
form: powder to crystal
color: White to Light yellow to Light orange
CAS DataBase Reference: 57103-21-6

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Safety

HS Code: 2933.99.8290

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical

Product number: D4543
Product name: 3,6-Diiodo-9-phenylcarbazole
Purity: >98.0%(GC)
Packaging: 1g
Price: $39
Updated: 2025/07/31

TCI Chemical

Product number: D4543
Product name: 3,6-Diiodo-9-phenylcarbazole
Purity: >98.0%(GC)
Packaging: 5g
Price: $201
Updated: 2025/07/31

TRC

Product number: D493243
Product name: 3,6-Diiodo-9-phenyl-9H-carbazole
Packaging: 100mg
Price: $60
Updated: 2021/12/16

TRC

Product number: D493243
Product name: 3,6-Diiodo-9-phenyl-9H-carbazole
Packaging: 500mg
Price: $155
Updated: 2021/12/16

Chem-Impex

Product number: 44419
Product name: 3,6-Diiodo-9-phenylcarbazole,≥98%(GC)
Purity: ≥98%(GC)
Packaging: 1G
Price: $43.87
Updated: 2021/12/16

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3,6-DIIODO-9-PHENYL-9H-CARBAZOLE Chemical Properties,Usage,Production

Synthesis

1150-62-5

57103-21-6

The general procedure for the synthesis of 3,6-diiodo-9-phenylcarbazole from N-phenylcarbazole was as follows: first, 24.3 g (100 mmol) of 9-phenylcarbazole was dissolved in 700 mL of glacial acetic acid, followed by the slow addition of 44.9 g (200 mmol) of N-iodosuccinimide. The reaction mixture was stirred at room temperature overnight. Upon completion of the reaction, the resulting precipitate was collected by filtration and the residue was washed sequentially with saturated aqueous sodium bicarbonate solution, water and methanol and finally dried. 47.0 g (95% yield) of the target product 3,6-diiodo-9-phenylcarbazole was obtained as a white powder.

References

[1] Patent: WO2006/70912, 2006, A1. Location in patent: Page/Page column 58; 59
[2] Patent: WO2006/43647, 2006, A1. Location in patent: Page/Page column 59-60
[3] Patent: WO2012/25510, 2012, A1. Location in patent: Page/Page column 23
[4] Patent: EP2433928, 2012, A1. Location in patent: Page/Page column 16-17
[5] Journal of Chemical Research, 2017, vol. 41, # 2, p. 79 - 81

3,6-DIIODO-9-PHENYL-9H-CARBAZOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3,6-DIIODO-9-PHENYL-9H-CARBAZOLE manufacturers

Career Henan Chemical Co

Product: 3,6-DIIODO-9-PHENYL-9H-CARBAZOLE 57103-21-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 1ton
Release date: 2018-08-06

57103-21-6, 3,6-DIIODO-9-PHENYL-9H-CARBAZOLERelated Search:

3,6-DIIODO-9-PHENYL-9H-CARBAZOLE

3,6-Diiodo-9-phenylcarbazole

9H-Carbazole,3,6-diiodo-9-phenyl

3,6-Diiodo-9-phenylcarbazole&gt

57103-21-6

C18H11I2N