4-(HYDROXYMETHYL)PHENYL PIVALATE

Product Name: 4-(HYDROXYMETHYL)PHENYL PIVALATE
CAS No.: 59012-91-8
Chemical Name: 4-(HYDROXYMETHYL)PHENYL PIVALATE
Synonyms: 4-(HydroxyMethyl)phenol pivalate;4-(HYDROXYMETHYL)PHENYL PIVALATE;Propanoic acid, 2,2-dimethyl-, 4-(hydroxymethyl)phenyl ester
CBNumber: CB32459737
Molecular Formula: C12H16O3
Formula Weight: 208.25
MOL File: 59012-91-8.mol

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4-(HYDROXYMETHYL)PHENYL PIVALATE Property

storage temp.: Sealed in dry,Room Temperature

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: CHM0390055
Product name: 4-(HYDROXYMETHYL)PHENYL PIVALATE
Purity: 95.00%
Packaging: 5MG
Price: $505.4
Updated: 2021/12/16

AK Scientific

Product number: 8773AB
Product name: 4-(Hydroxymethyl)phenylpivalate
Packaging: 100mg
Price: $273
Updated: 2021/12/16

Alichem

Product number: 59012918
Product name: 4-(Hydroxymethyl)phenylpivalate
Packaging: 250mg
Price: $279.84
Updated: 2021/12/16

Crysdot

Product number: CD12057922
Product name: 4-(Hydroxymethyl)phenylpivalate
Purity: 95+%
Packaging: 1g
Price: $653
Updated: 2021/12/16

Alichem

Product number: 59012918
Product name: 4-(Hydroxymethyl)phenylpivalate
Packaging: 1g
Price: $693
Updated: 2021/12/16

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4-(HYDROXYMETHYL)PHENYL PIVALATE Chemical Properties,Usage,Production

Synthesis

623-05-2

3282-30-2

59012-91-8

Procedure for the synthesis of 4-(hydroxymethyl)phenyl trimethyl acetate (Compound M1): to a stirred solution of 4-hydroxybenzyl alcohol (6.21 g, 50 mmol) in anhydrous THF (50 mL) was added triethylamine (10.43 mL, 75 mmol) under the protection of argon, followed by a slow dropwise addition of pivaloyl chloride (6.79 mL, 55 mmol) at room temperature. The reaction mixture was continued to be stirred at room temperature for 60 minutes. Upon completion of the reaction, the reaction was quenched by the addition of water (0.2 mL) and the mixture was allowed to stand overnight. Subsequently, the reaction mixture was diluted with EtOAc (~400 mL) and washed sequentially with saturated NaHCO3 solution (3 x 100 mL) and brine (100 mL). The organic phase was dried with Na2SO4, filtered and concentrated. The product was purified by rapid chromatography on a silica gel column (4 × 20 cm) (TLC conditions: Rf = 0.4, unfolding agent was ethyl acetate/hexane (4:6)), and ethyl acetate/hexane (4:6) was used as eluent. The fractions containing the pure product were combined, concentrated and dried under vacuum to give 7.75 g (74% yield) of the target compound in the form of a colorless oil.1H NMR (DMSO-d6): δ 7.35 (d, 2H, J = 8.6 Hz), 7.04 (d, 2H, J = 8.6 Hz), 5.22 (t, 1H), 4.50 (d, 2H), 1.31 (s, 9H).

References

[1] Journal of Organic Chemistry, 2005, vol. 70, # 23, p. 9470 - 9479
[2] Journal of Organic Chemistry, 2006, vol. 71, # 22, p. 8651 - 8654
[3] Chemical Communications, 2018, vol. 54, # 61, p. 8466 - 8469
[4] Patent: WO2015/153496, 2015, A1. Location in patent: Paragraph 00201
[5] Patent: WO2015/153510, 2015, A1. Location in patent: Paragraph 00201

4-(HYDROXYMETHYL)PHENYL PIVALATE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 4-(HYDROXYMETHYL)PHENYL PIVALATE manufacturers

Huida Pharmaceutical Technology (Shanghai) Co., Ltd.

Product: 4-(HYDROXYMETHYL)PHENYL PIVALATE 59012-91-8
Price: US $0.00-0.00/kg
Min. Order: 0.1kg
Purity: 98%
Supply Ability: 100kg
Release date: 2023-03-09

59012-91-8, 4-(HYDROXYMETHYL)PHENYL PIVALATERelated Search:

4-(HYDROXYMETHYL)PHENYL PIVALATE

4-(HydroxyMethyl)phenol pivalate

Propanoic acid, 2,2-dimethyl-, 4-(hydroxymethyl)phenyl ester

59012-91-8