ChemicalBook > CAS DataBase List > Ethyl 2-amino-1-methyl-1H-imidazole-5-carboxylate

Ethyl 2-amino-1-methyl-1H-imidazole-5-carboxylate

Product Name
Ethyl 2-amino-1-methyl-1H-imidazole-5-carboxylate
CAS No.
177760-04-2
Chemical Name
Ethyl 2-amino-1-methyl-1H-imidazole-5-carboxylate
Synonyms
ethyl 2-aMino-1-Methyl-1H-iMidazole-5-carboxylate;EOS-61727;ethyl 2-amino-3-methylimidazole-4-carboxylate;2-Amino-3-methyl-3H-imidazole-4-carboxylic acid;Ethyl 2-aMino-3-Methyl-3H-iMidazole-4-carboxylate;ethyl 2-amino-1-N-methyl-1H-imidazole-5-carboxylate;2-amino-3-methyl-4-imidazolecarboxylic acid ethyl ester;2-Amino-1-methyl-1H-imidazole-5-carboxylic acid ethyl ester;2-AMINO-3-METHYL-3H-IMIDAZOLE-4-CARBOXYLIC ACID ETHYL ESTER;2-AMINO-3-METHYL-3H-IMIDAZOLE-4-CARBOXYLIC ACID ETHYL ESTER-4
CBNumber
CB32459858
Molecular Formula
C7H11N3O2
Formula Weight
169.18
MOL File
177760-04-2.mol
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Ethyl 2-amino-1-methyl-1H-imidazole-5-carboxylate Property

Boiling point:
338.2±34.0 °C(Predicted)
Density 
1.29
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
5.83±0.25(Predicted)
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Safety

HS Code 
2933299090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B440568
Product name
ethyl2-amino-1-methyl-1H-imidazole-5-carboxylate
Packaging
50mg
Price
$45
Updated
2021/12/16
TRC
Product number
B440568
Product name
ethyl2-amino-1-methyl-1H-imidazole-5-carboxylate
Packaging
500mg
Price
$310
Updated
2021/12/16
ChemScene
Product number
CS-M2111
Product name
1H-Imidazole-5-carboxylicacid,2-amino-1-methyl-,ethylester
Packaging
5g
Price
$408
Updated
2021/12/16
Apolloscientific
Product number
OR963687
Product name
2-Amino-3-methyl-3H-imidazole-4-carboxylicacidethylester
Purity
98%
Packaging
1g
Price
$185
Updated
2021/12/16
AK Scientific
Product number
Z4300
Product name
Ethyl2-amino-1-methyl-1H-imidazole-5-carboxylate
Packaging
1g
Price
$208
Updated
2021/12/16
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Ethyl 2-amino-1-methyl-1H-imidazole-5-carboxylate Chemical Properties,Usage,Production

Synthesis

A solution of N-formyl sarcosine ethyl ester in an equal mixture of ethyl formate and THF with cyclohexane was added slowly to NaH (60% wt in mineral oil) at RT. After that, the hydrogen release stopped, and the reaction mixture was unde-stirred for 3.5 h. The reaction mixture was concentrated under a vacuum and then suspended in a solution of EtOH containing concentrated aq.HCl 32%. After refluxing for 2 h, the hot reaction mixture was filtered and the resulting solid was washed with boiling EtOH. The filtrate was concentrated under vacuum and diluted with a mixture of EtOH/water. The pH was adjusted to 3, using an aqueous 5M solution of NaOH, and cyanamide was added. The resulting mixture was refluxed for 1.5 h, then cooled to rt and concentrated under reduced pressure to approximately 1/8 of the initial volume. The pH of the remaining solution was adjusted to 9-10 with a saturated aqueous solution of potassium carbonate, after cooling in an ice-water bath. The precipitate formed was removed by filtration, washed with water, and dried under vacuum at 40 °C overnight to afford Ethyl 2-amino-1-methyl-1H-imidazole-5-carboxylate as a pale yellow to orange solid.

Ethyl 2-amino-1-methyl-1H-imidazole-5-carboxylate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Ethyl 2-amino-1-methyl-1H-imidazole-5-carboxylate manufacturers

Career Henan Chemical Co
Product
2-AMINO-3-METHYL-3H-IMIDAZOLE-4-CARBOXYLIC ACID ETHYL ESTER 177760-04-2
Price
US $1.00/KG
Min. Order
1KG
Purity
97%-99.9%
Supply Ability
200kg
Release date
2020-03-05

177760-04-2, Ethyl 2-amino-1-methyl-1H-imidazole-5-carboxylateRelated Search:

Ethyl 2-amino-1-methyl-1H-imidazole-5-carboxylate ETHYL 2-AMINO-1-METHYLIMIDAZOLE-5-CARBOXYLATE HYDROCHLORIDE METHYL 2-METHOXYMETHYL-IMIDAZO[1,2-A]PYRIMIDINE 3-CARBOXYLATE ETHYL 2-METHYL-IMIDAZO[1,2-A]PYRIMIDINE 3-CARBOXYLATE ETHYL 2-ISOPROPYL-IMIDAZO[1,2-A]PYRIMIDINE 3-CARBOXYLATE ETHYL 2-CYCLOPENTYLETHYL-IMIDAZO[1,2-A]PYRIMIDINE 3-CARBOXYLATE ETHYL 2-(TRIFLUOROMETHYL)IMIDAZO[1,2-A]PYRIMIDINE-3-CARBOXYLATE ETHYL IMIDAZO[1,2-A]PYRIMIDINE-3-CARBOXYLATE

  • 2-AMINO-3-METHYL-3H-IMIDAZOLE-4-CARBOXYLIC ACID ETHYL ESTER
  • Ethyl 2-aMino-3-Methyl-3H-iMidazole-4-carboxylate
  • 2-Amino-1-methyl-1H-imidazole-5-carboxylic acid ethyl ester
  • ethyl 2-aMino-1-Methyl-1H-iMidazole-5-carboxylate
  • 1H-IMidazole-5-carboxylic acid, 2-aMino-1-Methyl-, ethyl ester
  • 2-AMINO-3-METHYL-3H-IMIDAZOLE-4-CARBOXYLIC ACID ETHYL ESTER-4
  • ethyl 2-amino-3-methylimidazole-4-carboxylate
  • EOS-61727
  • 2-amino-3-methyl-4-imidazolecarboxylic acid ethyl ester
  • ethyl 2-amino-1-N-methyl-1H-imidazole-5-carboxylate
  • 2-Amino-3-methyl-3H-imidazole-4-carboxylic acid
  • 177760-04-2