ChemicalBook > CAS DataBase List > 4-BROMO-2-THIOPHENECARBOXAMIDE

4-BROMO-2-THIOPHENECARBOXAMIDE

Product Name
4-BROMO-2-THIOPHENECARBOXAMIDE
CAS No.
83933-17-9
Chemical Name
4-BROMO-2-THIOPHENECARBOXAMIDE
Synonyms
4-bromothiophene-2-carboxamide;4-BROMO-2-THIOPHENECARBOXAMIDE;2-thiophenecarboxamide, 4-bromo-;4-bromo-2-thiophenecarboxamide(SALTDATA: FREE)
CBNumber
CB32460979
Molecular Formula
C5H4BrNOS
Formula Weight
206.06
MOL File
83933-17-9.mol
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4-BROMO-2-THIOPHENECARBOXAMIDE Property

storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
Appearance
White to off-white Solid
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Safety

Risk Statements 
43
Safety Statements 
36/37
HazardClass 
IRRITANT
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H317May cause an allergic skin reaction

H319Causes serious eye irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B698985
Product name
4-Bromothiophene-2-carboxamide
Packaging
250mg
Price
$70
Updated
2021/12/16
TRC
Product number
B698985
Product name
4-Bromothiophene-2-carboxamide
Packaging
1g
Price
$155
Updated
2021/12/16
AK Scientific
Product number
V7917
Product name
4-Bromothiophene-2-carboxamide
Packaging
10g
Price
$563
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0098880
Product name
4-BROMOTHIOPHENE-2-CARBOXAMIDE
Purity
95.00%
Packaging
1G
Price
$764.03
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0098880
Product name
4-BROMOTHIOPHENE-2-CARBOXAMIDE
Purity
95.00%
Packaging
5G
Price
$1334.03
Updated
2021/12/16
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4-BROMO-2-THIOPHENECARBOXAMIDE Chemical Properties,Usage,Production

Synthesis

31767-01-8

83933-17-9

The general procedure for the synthesis of 4-bromothiophene-2-carboxamide from the compound (CAS: 31767-01-8) is as follows: in a 25 mL round-bottomed flask equipped with a magnetic stirrer, aldoxime (5 mmol), copper(II) acetate (45 mg, 0.25 mmol), acetonitrile (10 mg, 0.25 mmol), and ethanol (15 mL) were added in sequence. The reaction mixture was stirred for 4-8 hours at 78 °C or 12 hours at room temperature. After completion of the reaction, the solvent was removed by rotary evaporator. The crude product was purified by column chromatography to afford the target compound 4-bromothiophene-2-carboxamide.

References

[1] RSC Advances, 2016, vol. 6, # 43, p. 37093 - 37098
[2] Journal of Chemical Research, 2016, vol. 40, # 10, p. 594 - 596
[3] Bulletin de la Societe Chimique de France, 1967, p. 4115 - 4120

4-BROMO-2-THIOPHENECARBOXAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-BROMO-2-THIOPHENECARBOXAMIDE Suppliers

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83933-17-9, 4-BROMO-2-THIOPHENECARBOXAMIDERelated Search:


  • 4-BROMO-2-THIOPHENECARBOXAMIDE
  • 4-bromothiophene-2-carboxamide
  • 2-thiophenecarboxamide, 4-bromo-
  • 4-bromo-2-thiophenecarboxamide(SALTDATA: FREE)
  • 83933-17-9