ChemicalBook > CAS DataBase List > 1-ACETYL-4-BOCAMINO-PIPERIDINE

1-ACETYL-4-BOCAMINO-PIPERIDINE

Product Name: 1-ACETYL-4-BOCAMINO-PIPERIDINE
CAS No.: 283167-28-2
Chemical Name: 1-ACETYL-4-BOCAMINO-PIPERIDINE
Synonyms: 1-ACETYL-4-BOCAMINO-PIPERIDINE;1-Acetyl-4-Boc-amino-piperidine, 97.5%;tert-butyl 1-acetylpiperidin-4-ylcarbamate;tert-butyl N-(1-acetyl-4-piperidyl)carbamate;tert-butyl N-(1-acetylpiperidin-4-yl)carbaMate;(1-Acetyl-4-piperidinyl)carbamic acid 1,1-dimethylethyl ester;Carbamic acid, N-(1-acetyl-4-piperidinyl)-, 1,1-dimethylethyl ester
CBNumber: CB32466476
Molecular Formula: C12H22N2O3
Formula Weight: 242.31
MOL File: 283167-28-2.mol

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1-ACETYL-4-BOCAMINO-PIPERIDINE Property

Boiling point:: 392.9±31.0 °C(Predicted)
Density: 1.08±0.1 g/cm3(Predicted)
storage temp.: 2-8°C
pka: 12.09±0.20(Predicted)
Appearance: White to off-white Solid

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Safety

Risk Statements: 20/21/22
Safety Statements: 23-24/25
HS Code: 29333990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: A145120
Product name: 1-Acetyl-(4-BOC-amino)piperidine
Packaging: 2.5g
Price: $215
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H48-1-0B
Product name: tert-Butyl N-(1-acetylpiperidin-4-yl)carbamate
Purity: 98.0%
Packaging: 5G
Price: $252
Updated: 2021/12/16

Oakwood

Product number: 046330
Product name: 1-Acetyl-4-boc-amino-piperidine
Purity: 98%
Packaging: 1g
Price: $33
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H48-1-0B
Product name: tert-Butyl N-(1-acetylpiperidin-4-yl)carbamate
Purity: 98.0%
Packaging: 1g
Price: $79
Updated: 2021/12/16

AK Scientific

Product number: 5271DA
Product name: Tert-Butyl(1-acetylpiperidin-4-yl)carbamate
Packaging: 25g
Price: $471
Updated: 2021/12/16

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1-ACETYL-4-BOCAMINO-PIPERIDINE Chemical Properties,Usage,Production

Synthesis

108-24-7

73874-95-0

283167-28-2

4-tert-butoxycarbonylaminopiperidine (5.0 g, 25 mmol) was dissolved in dichloromethane (80 mL) at 0 °C and triethylamine (3.8 g, 38 mmol) and acetic anhydride (2.6 g, 25 mmol) were added sequentially. The reaction mixture was stirred continuously at 0 °C for 2 hours. Upon completion of the reaction, the reaction was quenched by the addition of water (30 mL) and the organic phase was separated and washed with saturated sodium bicarbonate solution (30 mL). The organic layer was dried over anhydrous sodium sulfate and concentrated under reduced pressure to give tert-butyl (1-methylpiperidin-4-yl)carbamate (5.6 g, 93% yield) as a light yellow solid.LC-MS analysis: retention time 1.88 min; mass-to-charge ratio 265.1 [M+Na]+.

References

[1] Patent: WO2016/34673, 2016, A1. Location in patent: Page/Page column 91
[2] Patent: WO2016/34675, 2016, A1. Location in patent: Page/Page column 68
[3] Patent: WO2017/153520, 2017, A1. Location in patent: Page/Page column 64
[4] Patent: US2008/227780, 2008, A1. Location in patent: Page/Page column 53-54
[5] Patent: WO2015/198229, 2015, A1. Location in patent: Page/Page column 21

1-ACETYL-4-BOCAMINO-PIPERIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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1-ACETYL-4-BOCAMINO-PIPERIDINE Suppliers

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283167-28-2, 1-ACETYL-4-BOCAMINO-PIPERIDINERelated Search:

1-ACETYL-4-BOCAMINO-PIPERIDINE

(1-Acetyl-4-piperidinyl)carbamic acid 1,1-dimethylethyl ester

tert-butyl N-(1-acetylpiperidin-4-yl)carbaMate

1-Acetyl-4-Boc-amino-piperidine, 97.5%

tert-butyl 1-acetylpiperidin-4-ylcarbamate

Carbamic acid, N-(1-acetyl-4-piperidinyl)-, 1,1-dimethylethyl ester

tert-butyl N-(1-acetyl-4-piperidyl)carbamate

283167-28-2