3-Bromoindole-5-carboxylic Acid
- Product Name
- 3-Bromoindole-5-carboxylic Acid
- CAS No.
- 916179-87-8
- Chemical Name
- 3-Bromoindole-5-carboxylic Acid
- Synonyms
- 3-Bromoindole-5-carboxylic Acid;3-Bromo-1H-indole-5-carboxylicacid;1H-Indole-5-carboxylic acid, 3-bromo-
- CBNumber
- CB32500783
- Molecular Formula
- C9H6BrNO2
- Formula Weight
- 240.05
- MOL File
- 916179-87-8.mol
3-Bromoindole-5-carboxylic Acid Property
- Density
- 1.838
- storage temp.
- 2-8°C
- Appearance
- Off-white to light brown Solid
N-Bromosuccinimide Price
- Product number
- B688988
- Product name
- 3-Bromoindole-5-carboxylicacid
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
- Product number
- V9109
- Product name
- 3-Bromoindole-5-carboxylicacid
- Packaging
- 1g
- Price
- $142
- Updated
- 2021/12/16
- Product number
- HCH0316498
- Product name
- 3-BROMOINDOLE-5-CARBOXYLIC ACID
- Purity
- 96.00%
- Packaging
- 1G
- Price
- $203.7
- Updated
- 2021/12/16
- Product number
- HCH0316498
- Product name
- 3-BROMOINDOLE-5-CARBOXYLIC ACID
- Purity
- 96.00%
- Packaging
- 25G
- Price
- $1865.33
- Updated
- 2021/12/16
- Product number
- CM256576
- Product name
- 3-Bromoindole-5-carboxylicAcid
- Purity
- 95%
- Packaging
- 10g
- Price
- $256
- Updated
- 2021/12/16
3-Bromoindole-5-carboxylic Acid Chemical Properties,Usage,Production
Synthesis
1670-81-1
916179-87-8
General procedure for the synthesis of 3-bromoindole-5-carboxylic acid from indole-5-carboxylic acid: to a solution of indole-5-carboxylic acid (1.0 g, 6.2 mmol) in N,N-dimethylformamide (DMF, 10 mL) was added bromine (Br2, 334 μL, 1.05 eq.) and the reaction was carried out at room temperature (see Scheme 9). After the reaction was complete (about 5 min), the reaction mixture was poured into ice-cold sodium sulfite (Na2SO3, 1% aqueous solution, 100 mL) to precipitate the product. The precipitate was collected by filtration and dried under high vacuum. The resulting product was a light beige solid (1.46 g, 98% yield) and could be used in subsequent reactions without further purification. The structure of the product was confirmed by 1H NMR (DMSO-d6): δ 7.47 (d, 1H, J = 8.6 Hz), 7.65 (d, 1H, J = 2.5 Hz), 7.76 (dd, 1H, J = 7.3, 1.3 Hz), 8.04 (s, 1H), 11.77 (s, 1H), 12.57 (s, 1H).
References
[1] Patent: WO2006/125324, 2006, A1. Location in patent: Page/Page column 94-95
3-Bromoindole-5-carboxylic Acid Preparation Products And Raw materials
Raw materials
Preparation Products
3-Bromoindole-5-carboxylic Acid Suppliers
- Tel
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- Fax
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- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
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View Lastest Price from 3-Bromoindole-5-carboxylic Acid manufacturers
- Product
- 3-Bromoindole-5-carboxylic Acid 916179-87-8
- Price
- US $0.01/KG
- Min. Order
- 1KG
- Purity
- 98%; 99%
- Supply Ability
- 1kg; 10kg; 25kg
- Release date
- 2020-01-07