ChemicalBook > CAS DataBase List > Butyl Cyclopropanesulfonate

Butyl Cyclopropanesulfonate

Product Name
Butyl Cyclopropanesulfonate
CAS No.
83635-12-5
Chemical Name
Butyl Cyclopropanesulfonate
Synonyms
Cyclopropanesulfonic Acid Butyl Ester;Butyl Cyclopropanesulfonate
CBNumber
CB32502929
Molecular Formula
C7H14O3S
Formula Weight
178.25
MOL File
83635-12-5.mol
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Butyl Cyclopropanesulfonate Property

storage temp. 
Sealed in dry,Room Temperature
solubility 
Chloroform, Dichloromethane, Ethyl Acetate
form 
Oil
color 
Colourless
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Safety

HS Code 
2904100090
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC
Product number
B690730
Product name
ButylCyclopropanesulfonate
Packaging
1g
Price
$45
Updated
2021/12/16
TRC
Product number
B690730
Product name
ButylCyclopropanesulfonate
Packaging
2g
Price
$60
Updated
2021/12/16
TRC
Product number
B690730
Product name
ButylCyclopropanesulfonate
Packaging
5G
Price
$130
Updated
2021/12/16
TRC
Product number
B690730
Product name
ButylCyclopropanesulfonate
Packaging
10g
Price
$205
Updated
2021/12/16
TRC
Product number
B690730
Product name
ButylCyclopropanesulfonate
Packaging
25g
Price
$415
Updated
2021/12/16
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Butyl Cyclopropanesulfonate Chemical Properties,Usage,Production

Chemical Properties

Colourless Oil

Synthesis

139631-62-2

71-36-3

83635-12-5

Step A: Synthesis of Butyl Cyclopropanesulfonate: Cyclopropanesulfonyl chloride (5 g, 35 mmol, 1 eq.) was dissolved in excess n-butanol (20 mL). The reaction mixture was cooled to -10 °C and pyridine (5.8 mL, 70 mmol, 2 eq.) was added slowly and dropwise. Subsequently, the mixture was gradually warmed to room temperature and stirred overnight. Upon completion of the reaction, the solvent was removed by distillation under reduced pressure. The resulting white solid was dissolved in chloroform (CHCl3), and the organic phase was washed sequentially with water and saturated brine and dried over anhydrous magnesium sulfate (MgSO4). The organic phase was concentrated to give the oily product butyl cyclopropanesulfonate (4.8 g, 24.9 mmol, 71% yield). The product was characterized by 1H NMR (300 MHz, CDCl3): δ 4.25 (t, 2H), 2.46 (m, 1H), 1.74 (m, 2H), 1.45 (m, 2H), 1.25 (dd, 2H), 1.09 (dd, 2H), 0.93 (t, 3H).

References

[1] Patent: WO2010/145197, 2010, A1. Location in patent: Page/Page column 54-55
[2] Patent: US2015/368238, 2015, A1. Location in patent: Paragraph 0632; 0633
[3] Patent: WO2007/14011, 2007, A2. Location in patent: Page/Page column 51
[4] Patent: WO2013/178581, 2013, A1. Location in patent: Page/Page column 39; 40

Butyl Cyclopropanesulfonate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Butyl Cyclopropanesulfonate manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
Butyl cyclopropanesulfonate 83635-12-5
Price
US $1.00-0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100000KG
Release date
2020-01-10

83635-12-5, Butyl CyclopropanesulfonateRelated Search:


  • Butyl Cyclopropanesulfonate
  • Cyclopropanesulfonic Acid Butyl Ester
  • 83635-12-5
  • Intermediates
  • Miscellaneous Reagents
  • Sulfur & Selenium Compounds