5-(benzyloxy)-2,4-dichloropyrimidine

Product Name: 5-(benzyloxy)-2,4-dichloropyrimidine
CAS No.: 91183-17-4
Chemical Name: 5-(benzyloxy)-2,4-dichloropyrimidine
Synonyms: 5-(benzyloxy)-2,4-dichloropyrimidine;2,4-Dichloro-5-(Benzyloxy)pyrimidine;2,4-Dichloro-5-(phenylmethoxy)pyrimidine;Pyrimidine, 2,4-dichloro-5-(phenylmethoxy)-
CBNumber: CB32513732
Molecular Formula: C11H8Cl2N2O
Formula Weight: 255.1
MOL File: 91183-17-4.mol

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5-(benzyloxy)-2,4-dichloropyrimidine Property

Boiling point:: 381.6±27.0 °C(Predicted)
Density: 1.382
storage temp.: Inert atmosphere,Room Temperature
pka: -2.70±0.29(Predicted)
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific

Product number: 5228AC
Product name: 5-(Benzyloxy)-2,4-dichloropyrimidine
Packaging: 100mg
Price: $120
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0366679
Product name: 5-(BENZYLOXY)-2,4-DICHLOROPYRIMIDINE
Purity: 95.00%
Packaging: 5MG
Price: $495.62
Updated: 2021/12/16

Ambeed

Product number: A140504
Product name: 5-(Benzyloxy)-2,4-dichloropyrimidine
Purity: 98%
Packaging: 100mg
Price: $6
Updated: 2021/12/16

Ambeed

Product number: A140504
Product name: 5-(Benzyloxy)-2,4-dichloropyrimidine
Purity: 98%
Packaging: 250mg
Price: $13
Updated: 2021/12/16

Ambeed

Product number: A140504
Product name: 5-(Benzyloxy)-2,4-dichloropyrimidine
Purity: 98%
Packaging: 1g
Price: $36
Updated: 2021/12/16

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5-(benzyloxy)-2,4-dichloropyrimidine Chemical Properties,Usage,Production

Synthesis

92016-70-1

91183-17-4

Step 3: Compound 10c (8.9 g, 40 mmol) was added to 100 mL of phosphorus oxychloride (POCl3) and heated to reflux for 5 hours. Upon completion of the reaction, some of the phosphorous trichloride was removed by distillation. The reaction mixture was quenched by careful pouring into ice water. The pH of the mixture was adjusted to 7-8 with ammonia at a temperature below 10 °C. Subsequently, the mixture was extracted with ethyl acetate. The organic phases were combined, dried with anhydrous sodium sulfate and the solvent was concentrated under reduced pressure to give the target product 10d (1.7 g, 16.7% yield). Mass spectrometric analysis showed [M + H]+ of 255.1.

References

[1] Patent: EP2754659, 2014, A1. Location in patent: Paragraph 0168; 0173; 0174
[2] Patent: US2014/378488, 2014, A1. Location in patent: Paragraph 0380; 0385; 0386

5-(benzyloxy)-2,4-dichloropyrimidine Preparation Products And Raw materials

Raw materials

Preparation Products

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5-(benzyloxy)-2,4-dichloropyrimidine Suppliers

China 64 India 1 United States 4 Global 69

JinYan Chemicals(ShangHai) Co.,Ltd.

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AN PharmaTech Co Ltd

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View Lastest Price from 5-(benzyloxy)-2,4-dichloropyrimidine manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 2,4-Dichloro-5-(phenylmethoxy)pyrimidine 91183-17-4
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20T
Release date: 2020-05-15

Career Henan Chemical Co

Product: 5-(benzyloxy)-2,4-dichloropyrimidine 91183-17-4
Price: US $2.00/KG
Min. Order: 1g
Purity: 98%min
Supply Ability: ask
Release date: 2020-01-08

91183-17-4, 5-(benzyloxy)-2,4-dichloropyrimidineRelated Search:

5-(benzyloxy)-2,4-dichloropyrimidine

2,4-Dichloro-5-(phenylmethoxy)pyrimidine

2,4-Dichloro-5-(Benzyloxy)pyrimidine

Pyrimidine, 2,4-dichloro-5-(phenylmethoxy)-

91183-17-4