(2,3-dihydrobenzofuran-6-yl)methanol
- Product Name
- (2,3-dihydrobenzofuran-6-yl)methanol
- CAS No.
- 1083168-69-7
- Chemical Name
- (2,3-dihydrobenzofuran-6-yl)methanol
- Synonyms
- 4-Bromo-2,37-diaminopyridine;(2,3-Dihydrobenzofuran-6-yl);2,3-Dihydro-6-benzofuranmethanol;6-BenzofuranMethanol, 2,3-dihydro-;(2,3-dihydrobenzofuran-6-yl)methanol;2,3-dihydro-1-benzofuran-6-ylMethanol
- CBNumber
- CB32515978
- Molecular Formula
- C9H10O2
- Formula Weight
- 150.17
- MOL File
- 1083168-69-7.mol
(2,3-dihydrobenzofuran-6-yl)methanol Property
- Boiling point:
- 291.3±9.0 °C(Predicted)
- Density
- 1.217±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- pka
- 14.31±0.10(Predicted)
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B426640
- Product name
- (2,3-Dihydrobenzofuran-6-yl)methanol
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 5732AQ
- Product name
- 2,3-dihydro-1-benzofuran-6-ylmethanol
- Packaging
- 1g
- Price
- $1017.2
- Updated
- 2021/12/16
- Product number
- A136197
- Product name
- (2,3-Dihydrobenzofuran-6-yl)methanol
- Purity
- 98%
- Packaging
- 100mg
- Price
- $186
- Updated
- 2021/12/16
- Product number
- 61-5132
- Product name
- (2,3-dihydrobenzofuran-6-yl)methanol
- Purity
- 98%
- Packaging
- 0.1g
- Price
- $220
- Updated
- 2021/12/16
- Product number
- A136197
- Product name
- (2,3-Dihydrobenzofuran-6-yl)methanol
- Purity
- 98%
- Packaging
- 250mg
- Price
- $283
- Updated
- 2021/12/16
(2,3-dihydrobenzofuran-6-yl)methanol Chemical Properties,Usage,Production
Synthesis
1083168-68-6
1083168-69-7
Procedure: synthesis of (2,3-dihydrobenzofuran-6-yl)methanol; A THF solution of methyl 2,3-dihydrobenzofuran-6-carboxylate (17.8 g, 100 mmol) was slowly added to a stirred tetrahydrofuran (THF, 300 mL) solution of lithium aluminium hydride (6.1 g, 250 mmol) at 0 °C. The reaction mixture was continued to be stirred at room temperature for 1 hour. Upon completion of the reaction, the reaction was quenched by careful addition of saturated aqueous sodium hydroxide solution, followed by extraction of the mixture with ethyl acetate. The organic layers were combined, washed with saturated brine, dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to afford (2,3-dihydrobenzofuran-6-yl)methanol (13.8 g, 92.0% yield). The product was characterized by 1H NMR (400 MHz, CDCl3): δ 7.17 (d, J = 7.2 Hz, 1H), 6.84 (d, J = 7.2 Hz, 1H), 6.81 (s, 1H), 4.62 (s, 2H), 4.58 (t, J = 8.4 Hz, 2H), 3.20 (t, J = 8.4 Hz, 2H), 1.67 ( br s, 1H).
References
[1] Patent: WO2008/141119, 2008, A2. Location in patent: Page/Page column 77; 79
(2,3-dihydrobenzofuran-6-yl)methanol Preparation Products And Raw materials
Raw materials
Preparation Products
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