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6-Bromo-1-(tetrahydro-2H-pyran-4-yl)-1H-benzimidazole

Product Name
6-Bromo-1-(tetrahydro-2H-pyran-4-yl)-1H-benzimidazole
CAS No.
1245649-58-4
Chemical Name
6-Bromo-1-(tetrahydro-2H-pyran-4-yl)-1H-benzimidazole
Synonyms
6-bromo-1-(oxan-4-yl)benzimidazole;6-Bromo-1-(tetrahydro-2H-pyran-4-yl);6-Bromo-1-(tetrahydro-2H-pyran-4-yl)-1H-benzimidazole;1H-Benzimidazole, 6-bromo-1-(tetrahydro-2H-pyran-4-yl)-
CBNumber
CB32534674
Molecular Formula
C12H13BrN2O
Formula Weight
281.15
MOL File
1245649-58-4.mol
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6-Bromo-1-(tetrahydro-2H-pyran-4-yl)-1H-benzimidazole Property

Boiling point:
425.3±55.0 °C(Predicted)
Density 
1.60
storage temp. 
Inert atmosphere,Room Temperature
pka
4.10±0.10(Predicted)
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific
Product number
4647AA
Product name
6-Bromo-1-(tetrahydro-2H-pyran-4-yl)-1H-benzo[d]imidazole
Packaging
100mg
Price
$84
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0367685
Product name
6-BROMO-1-(TETRAHYDRO-2H-PYRAN-4-YL)-1H-BENZO[D]IMIDAZOLE
Purity
95.00%
Packaging
250MG
Price
$347.55
Updated
2021/12/16
Matrix Scientific
Product number
093302
Product name
6-Bromo-1-(tetrahydro-2H-pyran-4-yl)-1H-benzo[d]imidazole
Purity
95+%
Packaging
250mg
Price
$378
Updated
2021/12/16
Matrix Scientific
Product number
093302
Product name
6-Bromo-1-(tetrahydro-2H-pyran-4-yl)-1H-benzo[d]imidazole
Purity
95+%
Packaging
1g
Price
$807
Updated
2021/12/16
Ambeed
Product number
A116653
Product name
6-Bromo-1-(tetrahydro-2H-pyran-4-yl)-1H-benzo[d]imidazole
Purity
98%
Packaging
100mg
Price
$21
Updated
2021/12/16
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6-Bromo-1-(tetrahydro-2H-pyran-4-yl)-1H-benzimidazole Chemical Properties,Usage,Production

Synthesis

1162697-10-0

149-73-5

1245649-58-4

GENERAL STEPS: To a solution of trimethyl orthoformate (2 mL) of 5-bromo-N1-(tetrahydro-2H-pyran-4-yl)benzene-1,2-diamine (500 mg, 1.852 mmol) was added p-toluenesulfonic acid (TsOH, 15 mg, 0.0789 mmol). The reaction mixture was stirred at 100 °C for 12 hours. After completion of the reaction, the reaction mixture was extracted with dichloromethane (DCM), the organic layer was washed with water and then dried with anhydrous sodium sulfate. After filtration to remove the desiccant, the filtrate was concentrated and purified by column chromatography to give the crude product (201 mg, 38.53% yield).LCMS (m/z): 281.0, 283.0 ([M + H]+).

References

[1] Patent: WO2014/100695, 2014, A1. Location in patent: Paragraph 00344

6-Bromo-1-(tetrahydro-2H-pyran-4-yl)-1H-benzimidazole Preparation Products And Raw materials

Raw materials

Preparation Products

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6-Bromo-1-(tetrahydro-2H-pyran-4-yl)-1H-benzimidazole Suppliers

China 29 India 1 United Kingdom 1 United States 5 Global 36
Chiba Pharmaceutical Science and technology Co, Ltd.
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0531-81313138 13066006660
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QQ: 3366077777
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chibapharm@foxmail.com
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13120367189
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021-50315529
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China
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Shanghai Balmxy Pharmaceutical Co., Ltd
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021-24206007 13764915196
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Amadis Chemical Company Limited
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571-89925085
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0086-571-89925065
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Aikon International Limited
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3A Chemicals
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400-668-9898
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Shanghai Jizhi Biochemical Technology Co. Ltd.
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Henan Alpha Chemical Co., Ltd.
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0371-55055611 18137792234
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Career Henan Chemica Co
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1245649-58-4, 6-Bromo-1-(tetrahydro-2H-pyran-4-yl)-1H-benzimidazoleRelated Search:

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