ChemicalBook > CAS DataBase List > 952511-48-7 5-broMo-4-Methyl-1H-benzo[d]iMidazole

952511-48-7 5-broMo-4-Methyl-1H-benzo[d]iMidazole

Product Name
952511-48-7 5-broMo-4-Methyl-1H-benzo[d]iMidazole
CAS No.
952511-48-7
Chemical Name
952511-48-7 5-broMo-4-Methyl-1H-benzo[d]iMidazole
Synonyms
5-Bromo-4-methylbenzimidazole;5-Bromo-4-methyl-1H-benzimidazole;1H-Benzimidazole, 6-bromo-7-methyl-;6-bromo-7-methyl-1H-benzo[d]imidazole;5-broMo-4-Methyl-1H-benzo[d]iMidazole;5-Bromo-4-methyl-1H-benzimidazole 97%;952511-48-7 5-broMo-4-Methyl-1H-benzo[d]iMidazole
CBNumber
CB32552742
Molecular Formula
C8H7BrN2
Formula Weight
211.06
MOL File
952511-48-7.mol
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952511-48-7 5-broMo-4-Methyl-1H-benzo[d]iMidazole Property

Boiling point:
418.3±25.0 °C(Predicted)
Density 
1.654±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
11.60±0.30(Predicted)
Appearance
Yellow to brown Solid
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Safety

HS Code 
2933998090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

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N-Bromosuccinimide Price

TRC
Product number
B814643
Product name
5-bromo-4-methyl-1H-benzo[d]imidazole
Packaging
100mg
Price
$155
Updated
2021/12/16
SynQuest Laboratories
Product number
3H31-9-45
Product name
5-Bromo-4-methyl-1H-benzimidazole
Packaging
100mg
Price
$98
Updated
2021/12/16
AK Scientific
Product number
6383AC
Product name
5-Bromo-4-methyl-1H-benzo[d]imidazole
Packaging
250mg
Price
$154
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0367011
Product name
5-BROMO-4-METHYL-1H-BENZO[D]IMIDAZOLE
Purity
95.00%
Packaging
5MG
Price
$499.1
Updated
2021/12/16
Ambeed
Product number
A239929
Product name
5-Bromo-4-methyl-1H-benzo[d]imidazole
Purity
97%
Packaging
100mg
Price
$51
Updated
2021/12/16
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952511-48-7 5-broMo-4-Methyl-1H-benzo[d]iMidazole Chemical Properties,Usage,Production

Synthesis

64-18-6

952511-74-9

952511-48-7

3. A mixture of 4-bromo-3-methylbenzene-1,2-diamine (28 g, 140 mmol), formic acid (240 mL), and 37% hydrochloric acid (400 mL) was heated to 60 °C and held for 12 h. The reaction was completed by filtration. Upon completion of the reaction, the mixture was cooled in an ice-water bath and the pH was slowly adjusted to 8-9 with 28% ammonia. the resulting solid was collected by filtration, washed with water, and dried in air to afford 5-bromo-4-methyl-1H-benzo[d]imidazole (25 g, 98% yield) as a yellow solid. Mass spectrum (ESI) m/z = 213 [M + 1]+.

References

[1] Patent: WO2013/26914, 2013, A1. Location in patent: Page/Page column 143
[2] Patent: US2010/222345, 2010, A1. Location in patent: Page/Page column 87

952511-48-7 5-broMo-4-Methyl-1H-benzo[d]iMidazole Preparation Products And Raw materials

Raw materials

Preparation Products

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952511-48-7 5-broMo-4-Methyl-1H-benzo[d]iMidazole Suppliers

Shanghai Hanhong Scientific Co.,Ltd.
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