Furan, tetrahydro-3-iodo-, (3R)-
- Product Name
- Furan, tetrahydro-3-iodo-, (3R)-
- CAS No.
- 873063-62-8
- Chemical Name
- Furan, tetrahydro-3-iodo-, (3R)-
- Synonyms
- (3R)-3-Iodooxolane;Cholest-5-en-3-ol,(8α)-;(3R)-3-Iodotetrahydrofuran;(R)-3-Iodo-tetrahydrofuran;1-Butanesulfonicacid,8-hydroxy-;Furan, tetrahydro-3-iodo-, (3R)-
- CBNumber
- CB32552777
- Molecular Formula
- C4H7IO
- Formula Weight
- 198
- MOL File
- 873063-62-8.mol
Furan, tetrahydro-3-iodo-, (3R)- Property
- Boiling point:
- 187.0±33.0 °C(Predicted)
- Density
- 1.93±0.1 g/cm3(Predicted)
- storage temp.
- 2-8°C(protect from light)
- Appearance
- Colorless to light yellow Liquid
Safety
- HS Code
- 2932190090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- P000385396
- Product name
- (R)-3-Iodotetrahydrofuran
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $103
- Updated
- 2021/12/16
- Product number
- AS17263
- Product name
- (R)-3-Iodotetrahydrofuran
- Purity
- 96% ee
- Packaging
- 250mg
- Price
- $169
- Updated
- 2021/12/16
- Product number
- OR52586
- Product name
- (3R)-3-Iodotetrahydrofuran
- Packaging
- 250mg
- Price
- $218
- Updated
- 2021/12/16
- Product number
- P000385396
- Product name
- (R)-3-Iodotetrahydrofuran
- Purity
- 95+%
- Packaging
- 100mg
- Price
- $69
- Updated
- 2021/12/16
- Product number
- 2H10-H-19
- Product name
- (3R)-3-Iodotetrahydrofuran
- Packaging
- 250mg
- Price
- $240
- Updated
- 2021/12/16
Furan, tetrahydro-3-iodo-, (3R)- Chemical Properties,Usage,Production
Synthesis
918439-76-6
873063-62-8
The general procedure for the synthesis of (R)-3-iodotetrahydrofuran from (S)-3-iodotetrahydrofuran was as follows: to a solution of (S)-tetrahydrofuran-3-ol (983 mg, 11.16 mmol) in dichloromethane (50 mL) was added triphenylphosphine (5.0 g, 21.20 mmol), glyoxal (1.4 g, 21.20 mmol) and iodine (5.0 g, 21.20 mmol). The reaction mixture was refluxed overnight, cooled and the reaction was quenched with saturated sodium thiosulfate solution. The organic layer was separated, dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give a yellow solid. The solid was ground with hexane at room temperature for 2 h. The filtrate was concentrated after filtration. Finally, it was purified by silica gel column chromatography with ethyl acetate/hexane (0-5%) as eluent for 20 min to give (R)-3-iodotetrahydrofuran as a clear oil (1.0 g, 52% yield).
References
[1] Patent: WO2011/146287, 2011, A1. Location in patent: Page/Page column 120-121
Furan, tetrahydro-3-iodo-, (3R)- Preparation Products And Raw materials
Raw materials
Preparation Products
Furan, tetrahydro-3-iodo-, (3R)- Suppliers
- Tel
- 86-25-57062118
- Fax
- 86-25-57065896
- sales@jspsn.com
- Country
- China
- ProdList
- 496
- Advantage
- 57
- Tel
- 18270980682
- Fax
- 021 51613951
- mlcheng@sunwaypharm.cn
- Country
- China
- ProdList
- 8669
- Advantage
- 57
- Tel
- 18-086626237 18086626237
- Fax
- qq:2693528373
- 2693528373@qq.com
- Country
- China
- ProdList
- 2973
- Advantage
- 56
- Tel
- Fax
- -
- eric_feng1954@126.com
- Country
- China
- ProdList
- 9248
- Advantage
- 55
- Tel
- 15076683720
- Fax
- 022-23754520
- klq@cw-bio.com
- Country
- China
- ProdList
- 8011
- Advantage
- 55
- Tel
- 571-89925085
- Fax
- 0086-571-89925065
- sales@amadischem.com
- Country
- China
- ProdList
- 131957
- Advantage
- 58
- Tel
- 025-58859352 18068836627
- Fax
- 02557626880
- sales01@aikonchem.com
- Country
- China
- ProdList
- 16027
- Advantage
- 58
- Tel
- 4009004166/18616739031 18616739031
- 3007523370@qq.com
- Country
- China
- ProdList
- 52687
- Advantage
- 58
- Tel
- 微信 17321281695 18019252918
- Fax
- qq:1454668768
- 1454668768@qq.com
- Country
- China
- ProdList
- 14856
- Advantage
- 58
- Tel
- +86-023-6139-8061 +86-86-13650506873
- sales@chemdad.com
- Country
- China
- ProdList
- 39927
- Advantage
- 58
View Lastest Price from Furan, tetrahydro-3-iodo-, (3R)- manufacturers
- Product
- Furan, tetrahydro-3-iodo-, (3R)- 873063-62-8
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10000KGS
- Release date
- 2025-03-19