ChemicalBook > CAS DataBase List > α,β-1-Methyl-D-ribofuranoside

α,β-1-Methyl-D-ribofuranoside

Product Name: α,β-1-Methyl-D-ribofuranoside
CAS No.: 13039-63-9
Chemical Name: α,β-1-Methyl-D-ribofuranoside
Synonyms: (2R,3S,4R)-2-(Hydroxymethyl)-5-methoxytetrahydrofuran-3,4-diol;Methyl D-ribofuranoside(α and β mixture);AzacitidineImpurity46;α,β-1-Methyl-D-ribofuranoside;α,β-1-Methyl-D-ribofuranoside;(2R,3S,4R)-2-(Hydroxymethyl)-5-methoxytetrahydrofuran-3,4-diol(α and β mixture)
CBNumber: CB32603556
Molecular Formula: C6H12O5
Formula Weight: 164.16
MOL File: 13039-63-9.mol

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α,β-1-Methyl-D-ribofuranoside Property

storage temp.: Sealed in dry,Room Temperature
Stability:: Hygroscopic

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific

Product number: 5558AA
Product name: (2R,3S,4R)-2-(Hydroxymethyl)-5-methoxytetrahydrofuran-3,4-diol
Packaging: 5g
Price: $492
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CRB0005204
Product name: (2R,3S,4R)-2-(HYDROXYMETHYL)-5-METHOXYTETRAHYDROFURAN-3,4-DIOL
Purity: 95.00%
Packaging: 5MG
Price: $497.57
Updated: 2021/12/16

Ambeed

Product number: A134503
Product name: MethylD-ribofuranoside(αandβmixture)
Purity: 97%
Packaging: 25g
Price: $1236
Updated: 2021/12/16

Ambeed

Product number: A134503
Product name: MethylD-ribofuranoside(αandβmixture)
Purity: 97%
Packaging: 5g
Price: $1236
Updated: 2021/12/16

Ambeed

Product number: A134503
Product name: MethylD-ribofuranoside(αandβmixture)
Purity: 97%
Packaging: 250mg
Price: $113
Updated: 2021/12/16

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α,β-1-Methyl-D-ribofuranoside Chemical Properties,Usage,Production

Uses

Methyl D-Ribofuranoside is used in the preparation of antiviral nucleosides and derivatives thereof.

Synthesis

67-56-1

532-20-7

1824-96-0

General procedure for the synthesis of methyl α-D-xylofuranoside from methanol and 2-furancarboxylic acid (CAS:532-20-7): D-ribose (500 g, 3.33 mol) was dissolved in 1.5 L of anhydrous methanol containing 0.5% (v/v) hydrochloric acid, and the reaction system was placed in a round-bottomed flask fitted with a drying tube of calcium carbonate, and the reaction was stirred for 48 h at room temperature. Upon completion of the reaction, the pH of the reaction mixture was adjusted to 7 using Dowex (OH type) ion exchange resin to neutralize the acidity. Subsequently, the resin was removed by filtration, the filtrate was concentrated under reduced pressure to remove the solvent, and the resulting residue was dried under vacuum overnight to afford methyl α-D-xylofuranoside (550 g, 98% yield).

References

[1] European Journal of Organic Chemistry, 2006, # 14, p. 3152 - 3168
[2] Angewandte Chemie - International Edition, 2017, vol. 56, # 39, p. 11963 - 11965
[3] Angew. Chem., 2017, vol. 129, # 39, p. 12125 - 12127,3
[4] Tetrahedron, 1992, vol. 48, # 41, p. 9033 - 9072
[5] Patent: WO2005/27962, 2005, A1. Location in patent: Page/Page column 69-70

α,β-1-Methyl-D-ribofuranoside Preparation Products And Raw materials

Raw materials

Preparation Products

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13039-63-9, α,β-1-Methyl-D-ribofuranosideRelated Search:

α,β-1-Methyl-D-ribofuranoside

(2R,3S,4R)-2-(Hydroxymethyl)-5-methoxytetrahydrofuran-3,4-diol

Methyl D-ribofuranoside(α and β mixture)

(2R,3S,4R)-2-(Hydroxymethyl)-5-methoxytetrahydrofuran-3,4-diol(α and β mixture)

AzacitidineImpurity46

α,β-1-Methyl-D-ribofuranoside

13039-63-9