2-nitro-3-Methyl-benzeneacetic acid
- Product Name
- 2-nitro-3-Methyl-benzeneacetic acid
- CAS No.
- 18710-86-6
- Chemical Name
- 2-nitro-3-Methyl-benzeneacetic acid
- Synonyms
- 2-nitro-3-Methyl-benzeneacetic acid;2-(3-Methyl-2-nitrophenyl)acetic acid;Benzeneacetic acid, 3-Methyl-2-nitro-
- CBNumber
- CB32609684
- Molecular Formula
- C9H9NO4
- Formula Weight
- 195.17
- MOL File
- 18710-86-6.mol
2-nitro-3-Methyl-benzeneacetic acid Property
- Melting point:
- 154-155℃
- Boiling point:
- 348.1±27.0 °C(Predicted)
- Density
- 1.346±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- pka
- 3.95±0.10(Predicted)
- form
- crystals
- color
- White
Safety
- HS Code
- 2916399090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H318Causes serious eye damage
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- M224065
- Product name
- 3-Methyl-2-nitrophenylaceticAcid
- Packaging
- 500mg
- Price
- $220
- Updated
- 2021/12/16
- Product number
- 4754-1-W1
- Product name
- 3-Methyl-2-nitrophenylacetic acid
- Packaging
- 250mg
- Price
- $52
- Updated
- 2021/12/16
- Product number
- 4754-1-W1
- Product name
- 3-Methyl-2-nitrophenylacetic acid
- Packaging
- 1g
- Price
- $122
- Updated
- 2021/12/16
- Product number
- 9227CU
- Product name
- 2-(3-Methyl-2-nitrophenyl)aceticacid
- Packaging
- 1g
- Price
- $182
- Updated
- 2021/12/16
- Product number
- 169237
- Product name
- 3-Methyl-2-nitrophenylacetic acid
- Packaging
- 1g
- Price
- $226
- Updated
- 2021/12/16
2-nitro-3-Methyl-benzeneacetic acid Chemical Properties,Usage,Production
Synthesis
91192-25-5
18710-86-6
General procedure for the synthesis of 2-(3-methyl-2-nitrophenyl)acetic acid from 2-(3-methyl-2-nitrophenyl)acetonitrile: 0.1 g (0.5 mmol) of 2-(3-methyl-2-nitrophenyl)acetonitrile and 0.4 mL of water were added to a 2-hour vial. Under stirring, 0.5 mL of concentrated hydrochloric acid was slowly added dropwise to this reaction slurry, followed by 50 drops of acetic acid. The reaction mixture was heated to 90°C and maintained at this temperature for 5 hours. Upon completion of the reaction, the solution was cooled and the formation of a white precipitate was observed. The white precipitate was collected by filtration, washed with water and dried to give 0.076 g (70% yield) of light yellow crystals. Mass spectrometry analysis (APCI) showed 195 [M-H]-.
References
[1] Patent: WO2004/41793, 2004, A1. Location in patent: Page 64
[2] Synthesis, 1987, # 5, p. 514 - 515
2-nitro-3-Methyl-benzeneacetic acid Preparation Products And Raw materials
Raw materials
Preparation Products
2-nitro-3-Methyl-benzeneacetic acid Suppliers
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