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6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one

Product Name
6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one
CAS No.
32263-70-0
Chemical Name
6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one
Synonyms
6-benzyloxytetralone;oxy)-3,4-dihydronaphthaL;6-Benzyloxy-3,4-dihydro-2H-naphthalen-1-one;6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one;6-(Benzyloxy)-3,4-dihydro-1(2H)-naphthalenone;6-phenylmethoxy-3,4-dihydro-2H-naphthalen-1-one;6-(benzyloxy)-1,2,3,4-tetrahydronaphthalen-1-one;1(2H)-Naphthalenone, 3,4-dihydro-6-(phenylMethoxy)-
CBNumber
CB32610013
Molecular Formula
C17H16O2
Formula Weight
252.31
MOL File
32263-70-0.mol
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6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one Property

Melting point:
96-99 °C(Solv: cyclohexane (110-82-7))
Boiling point:
433.4±34.0 °C(Predicted)
Density 
1.160±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
Appearance
Light brown to brown Solid
InChI
InChI=1S/C17H16O2/c18-17-8-4-7-14-11-15(9-10-16(14)17)19-12-13-5-2-1-3-6-13/h1-3,5-6,9-11H,4,7-8,12H2
InChIKey
SAYPPJQQGVXKAP-UHFFFAOYSA-N
SMILES
C1(=O)C2=C(C=C(OCC3=CC=CC=C3)C=C2)CCC1
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Biosynth Carbosynth
Product number
FB141115
Product name
6-(Benzyloxy)-3,4-dihydronaphthalen-1(2H)-one
Packaging
500mg
Price
$85
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB141115
Product name
6-(Benzyloxy)-3,4-dihydronaphthalen-1(2H)-one
Packaging
1g
Price
$135
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB141115
Product name
6-(Benzyloxy)-3,4-dihydronaphthalen-1(2H)-one
Packaging
2g
Price
$210
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB141115
Product name
6-(Benzyloxy)-3,4-dihydronaphthalen-1(2H)-one
Packaging
5G
Price
$410
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB141115
Product name
6-(Benzyloxy)-3,4-dihydronaphthalen-1(2H)-one
Packaging
10g
Price
$650
Updated
2021/12/16
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6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one Chemical Properties,Usage,Production

Synthesis

3470-50-6

100-39-0

32263-70-0

General procedure: 6-hydroxy-1-tetralone (0.3 g, 1.85 mmol) was suspended in acetone (15 mL) containing K2CO3 (3.70 mmol). Benzyl bromide (2.035 mmol) was added to the reaction mixture and heated under reflux conditions for 6 hours. The reaction process was monitored by silica gel thin layer chromatography (TLC) using ethyl acetate with petroleum ether (1:2) as mobile phase. Upon completion of the reaction, the mixture was filtered through a diatomaceous earth pad and the filtrate was subsequently concentrated under vacuum. The resulting crude product was purified by recrystallization from cyclohexane to give 6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one.

References

[1] Bioorganic and Medicinal Chemistry Letters, 2014, vol. 24, # 12, p. 2758 - 2763
[2] Bioorganic and Medicinal Chemistry Letters, 2014, vol. 24, # 12, p. 2758 - 2763
[3] Patent: US2018/155322, 2018, A1. Location in patent: Paragraph 1502; 1503
[4] European Journal of Organic Chemistry, 2003, # 15, p. 2799 - 2812
[5] Bioorganic and Medicinal Chemistry Letters, 2012, vol. 22, # 1, p. 144 - 148

6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one Preparation Products And Raw materials

Raw materials

Preparation Products

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6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one Suppliers

China 111 India 5 United Kingdom 1 United States 4 Global 121
A.J Chemicals
Tel
--
Fax
--
Email
sales@ajchem.in
Country
India
ProdList
6100
Advantage
58
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View Lastest Price from 6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one manufacturers

Hebei Chuanghai Biotechnology Co., Ltd
Product
6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one 32263-70-0
Price
US $0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
500000kg
Release date
2024-11-04
Career Henan Chemica Co
Product
6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one 32263-70-0
Price
US $9.80-8.00/KG
Min. Order
1KG
Purity
95%~99.99%
Supply Ability
10 MT/ Month
Release date
2020-10-28
Hebei Chuanghai Biotechnology Co,.LTD
Product
6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one 32263-70-0
Price
US $30.00-10.00/kg
Min. Order
10kg
Purity
99%
Supply Ability
100000kg
Release date
2024-08-14

32263-70-0, 6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-oneRelated Search:


  • 6-(Benzyloxy)-3,4-dihydro-1(2H)-naphthalenone
  • 6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one
  • 1(2H)-Naphthalenone, 3,4-dihydro-6-(phenylMethoxy)-
  • 6-Benzyloxy-3,4-dihydro-2H-naphthalen-1-one
  • oxy)-3,4-dihydronaphthaL
  • 6-phenylmethoxy-3,4-dihydro-2H-naphthalen-1-one
  • 6-(benzyloxy)-1,2,3,4-tetrahydronaphthalen-1-one
  • 6-benzyloxytetralone
  • 32263-70-0