5-AMino-6-iodo-pyridine-2-carbonitrile

Product Name: 5-AMino-6-iodo-pyridine-2-carbonitrile
CAS No.: 1079054-78-6
Chemical Name: 5-AMino-6-iodo-pyridine-2-carbonitrile
Synonyms: 5-AMino-6-Methylpicolinonitrile;3-Amino-6-cyano-2-methylpyridine;3-Amino-6-cyano-2-methylpyridine,95%;5-AMino-6-iodo-pyridine-2-carbonitrile;5-Amino-6-methyl-2-pyridinecarbonitrile;2-Pyridinecarbonitrile, 5-amino-6-methyl-
CBNumber: CB32629453
Molecular Formula: C7H7N3
Formula Weight: 133.15
MOL File: 1079054-78-6.mol

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5-AMino-6-iodo-pyridine-2-carbonitrile Property

Boiling point:: 361.0±42.0 °C(Predicted)
Density: 1.18±0.1 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 1.34±0.10(Predicted)
form: Solid
Appearance: Brown to reddish brown Solid

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Safety

HazardClass: 6.1
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: A898318
Product name: 5-Amino-6-methylpicolinonitrile
Packaging: 100mg
Price: $65
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H37-1-8C
Product name: 5-Amino-6-methylpicolinonitrile
Purity: 95%
Packaging: 1g
Price: $672
Updated: 2021/12/16

Apolloscientific

Product number: OR921514
Product name: 5-Amino-6-methylpicolinonitrile
Purity: 95%
Packaging: 1g
Price: $420
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0390618
Product name: 5-AMINO-6-METHYLPICOLINONITRILE
Purity: 95.00%
Packaging: 5MG
Price: $503.76
Updated: 2021/12/16

AK Scientific

Product number: Z3864
Product name: 5-Amino-6-methylpicolinonitrile
Packaging: 25g
Price: $536
Updated: 2021/12/16

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5-AMino-6-iodo-pyridine-2-carbonitrile Chemical Properties,Usage,Production

Synthesis

557-21-1

126325-47-1

1079054-78-6

The general procedure for the synthesis of 5-amino-6-methyl-2-cyanopyridine from zinc cyanide and 2-bromo-5-amino-6-methylpyridine was as follows: first, 6-cyano-2-methyl-3-aminopyridine was prepared; 3.5 g (18.6 mmol) of 6-bromo-2-methyl-3-aminopyridine, 352 mg (0.37 mmol) of tris(benzylideneacetone)dipalladium(0) , 532 mg (0.92 mmol) of 1,1 '-bis(diphenylphosphino)ferrocene, 146 mg (2.2 mmol) of zinc powder and 1.4 g (12 mmol) of zinc cyanide were mixed in 70 ml of N,N-dimethylacetamide. The reaction mixture was stirred at 20°C for 22 hours. After completion of the reaction, the reaction mixture was diluted with 200 ml of ethyl acetate and washed with 2N ammonium chloride solution. Note: Decantation was only possible after filtering the mixture on a Celite-type filter aid. The resulting organic phase was washed with sodium chloride solution, dried with magnesium sulfate and concentrated under reduced pressure. The evaporated residue was purified by silica gel chromatography using a dichloromethane/ethyl acetate mixture (9/1; v/v) as eluent, resulting in 1.6 g of 5-amino-6-methyl-2-cyanopyridine in the form of a yellow powder (yield = 65%). The melting point was 192-196 °C.

References

[1] Patent: US2007/54955, 2007, A1. Location in patent: Page/Page column 5
[2] Patent: WO2014/139150, 2014, A1. Location in patent: Page/Page column 55

5-AMino-6-iodo-pyridine-2-carbonitrile Preparation Products And Raw materials

Raw materials

Preparation Products

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5-AMino-6-iodo-pyridine-2-carbonitrile Suppliers

China 40 India 1 United States 4 Global 45

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1079054-78-6, 5-AMino-6-iodo-pyridine-2-carbonitrileRelated Search:

5-AMino-6-iodo-pyridine-2-carbonitrile

5-AMino-6-Methylpicolinonitrile

3-Amino-6-cyano-2-methylpyridine

5-Amino-6-methyl-2-pyridinecarbonitrile

2-Pyridinecarbonitrile, 5-amino-6-methyl-

3-Amino-6-cyano-2-methylpyridine,95%

1079054-78-6