ChemicalBook > CAS DataBase List > 3-BroMo-6-Methoxy-2-pyridinecarboxaldehyde

3-BroMo-6-Methoxy-2-pyridinecarboxaldehyde

Uses

Product Name: 3-BroMo-6-Methoxy-2-pyridinecarboxaldehyde
CAS No.: 269058-49-3
Chemical Name: 3-BroMo-6-Methoxy-2-pyridinecarboxaldehyde
Synonyms: 3-BROMO-6-METHOXYPICOLINALDEHYDE;3-bromo-2-formyl-6-methoxypyridine;3-Bromo-6-methoxy-pyridine-2-carbaldehyde;3-BroMo-6-Methoxy-2-pyridinecarboxaldehyde;2-Pyridinecarboxaldehyde, 3-bromo-6-methoxy-
CBNumber: CB32629903
Molecular Formula: C7H6BrNO2
Formula Weight: 216.03
MOL File: 269058-49-3.mol

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3-BroMo-6-Methoxy-2-pyridinecarboxaldehyde Property

Boiling point:: 253.3±35.0 °C(Predicted)
Density: 1.606±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: -0.16±0.10(Predicted)
Appearance: Off-white to light yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TRC

Product number: B429353
Product name: 3-bromo-6-methoxypicolinaldehyde
Packaging: 500mg
Price: $310
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB143420
Product name: 3-Bromo-6-methoxypicolinaldehyde
Packaging: 100mg
Price: $54
Updated: 2021/12/16

AK Scientific

Product number: Z4526
Product name: 3-Bromo-6-methoxypicolinaldehyde
Packaging: 100mg
Price: $89
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB143420
Product name: 3-Bromo-6-methoxypicolinaldehyde
Packaging: 250mg
Price: $107.5
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB143420
Product name: 3-Bromo-6-methoxypicolinaldehyde
Packaging: 500mg
Price: $185
Updated: 2021/12/16

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3-BroMo-6-Methoxy-2-pyridinecarboxaldehyde Chemical Properties,Usage,Production

Uses

3-bromo-6-methoxypicolinaldehyde is a useful research chemical.

Synthesis

623942-84-7

269058-49-3

Step F. Synthesis of 3-bromo-6-methoxy-2-pyridinecarboxaldehyde. A mixture of 3-bromo-2-hydroxymethyl-6-methoxypyridine (3.25 g, 14.9 mmol) and manganese dioxide (9.07 g, 104 mmol) in chloroform (50 mL) was heated to reflux for 18 hours. After completion of the reaction, the reaction mixture was filtered while hot and the filtrate was concentrated. The residue was purified by silica gel column chromatography (eluent: 10% ethyl acetate/hexane) to afford 3-bromo-6-methoxy-2-pyridinecarboxaldehyde (2.55 g, 80% yield). Mass spectrum (ESI): calculated value C7H6BrNO2, 214.96; measured value m/z 218.2 [M + H]+. 1H NMR (CDCl3): δ 10.13 (s, 1H), 7.80 (d, J = 8.7 Hz, 1H), 6.83 (d, J = 8.7 Hz, 1H), 3.99 (s, 3H).

References

[1] Tetrahedron Letters, 2000, vol. 41, # 12, p. 2007 - 2009
[2] Organic and Biomolecular Chemistry, 2003, vol. 1, # 16, p. 2865 - 2876
[3] Patent: US2006/287292, 2006, A1. Location in patent: Page/Page column 29
[4] Patent: US2016/75711, 2016, A1. Location in patent: Paragraph 0570; 0574

3-BroMo-6-Methoxy-2-pyridinecarboxaldehyde Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-BroMo-6-Methoxy-2-pyridinecarboxaldehyde manufacturers

Henan Fengda Chemical Co., Ltd

Product: 3-BroMo-6-Methoxy-2-pyridinecarboxaldehyde 269058-49-3
Price: US $8.00-1.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2024-04-03

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269058-49-3