2-DiMethylaMino-5-iodopyridine

Product Name: 2-DiMethylaMino-5-iodopyridine
CAS No.: 380381-36-2
Chemical Name: 2-DiMethylaMino-5-iodopyridine
Synonyms: 2-DiMethylaMino-5-iodopyridine;5-Iodo-N,N-diMethylpyridin-2-aMine;2-Pyridinamine, 5-iodo-N,N-dimethyl-;(5-Iodo-pyridin-2-yl)-dimethyl-amine
CBNumber: CB32671250
Molecular Formula: C7H9IN2
Formula Weight: 248.06
MOL File: 380381-36-2.mol

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2-DiMethylaMino-5-iodopyridine Property

storage temp.: Keep in dark place,Inert atmosphere,Room temperature
Appearance: White to yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H303May be harmfulif swallowed

H320Causes eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

AK Scientific

Product number: Z0561
Product name: 2-Dimethylamino-5-iodopyridine
Packaging: 100mg
Price: $103
Updated: 2021/12/16

AK Scientific

Product number: Z0561
Product name: 2-Dimethylamino-5-iodopyridine
Packaging: 1g
Price: $267
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0367500
Product name: 5-IODO-N,N-DIMETHYLPYRIDIN-2-AMINE
Purity: 95.00%
Packaging: 1G
Price: $825.3
Updated: 2021/12/16

AK Scientific

Product number: Z0561
Product name: 2-Dimethylamino-5-iodopyridine
Packaging: 5g
Price: $852
Updated: 2021/12/16

AOBChem

Product number: 23812
Product name: 2-Dimethylamino-5-iodopyridine
Purity: 97%
Packaging: 25g
Price: $1886
Updated: 2021/12/16

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2-DiMethylaMino-5-iodopyridine Chemical Properties,Usage,Production

Synthesis

280116-78-1

74-88-4

380381-36-2

2-(N-monomethylamino)-5-iodopyridine (99, 1.00 g, 4.27 mmol), potassium carbonate (2.95 g, 21.36 mmol) and iodomethane (145 mg, 8.546 mmol) were dissolved in dimethylacetamide (30 mL). The reaction mixture was heated at 90°C for 24 hours. Upon completion of the reaction, the reaction was terminated by the addition of water. The organic phase was extracted with ethyl acetate, dried over anhydrous sodium sulfate and concentrated under reduced pressure. The crude product was purified by column chromatography to afford 2-(N,N-dimethylamino)-5-iodopyridine (100, 603 mg, 57%).1H NMR (400 MHz, CDCl3) δ 3.08 (s, 6H), 6.34 (d, J = 8.4 Hz, 1H), 7.60 (dd, J = 8.8, 2.4 Hz, 1H), 8.27 (d, J = 2.4 Hz, 1H); 13C NMR (100 MHz, CDCl3) δ 38.1, 105.9, 107.1, 139.2, 148.3, 157.7.

References

[1] Patent: US2010/261727, 2010, A1. Location in patent: Page/Page column 23-24

2-DiMethylaMino-5-iodopyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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2-DiMethylaMino-5-iodopyridine Suppliers

China 39 India 1 United States 2 Global 42

Shanghai Jian Chao Chemical Technology Co., Ltd.

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380381-36-2