3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol

Product Name: 3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol
CAS No.: 1266084-47-2
Chemical Name: 3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol
Synonyms: 3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol;3,3-Dimethyl-6-Nitrobenzo[C][1,2]Oxaborol-1(3H)-Ol(WXC00403);1,3-dihydro-1-hydroxy-3,3-dimethyl-6-nitro-2,1-Benzoxaborole;2,1-Benzoxaborole, 1,3-dihydro-1-hydroxy-3,3-dimethyl-6-nitro-
CBNumber: CB32684496
Molecular Formula: C9H10BNO4
Formula Weight: 206.99
MOL File: 1266084-47-2.mol

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3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol Property

storage temp.: Store at room temperature
Appearance: White to off-white Solid
InChI: InChI=1S/C9H10BNO4/c1-9(2)7-4-3-6(11(13)14)5-8(7)10(12)15-9/h3-5,12H,1-2H3
InChIKey: MUNRAMHQIFHFBM-UHFFFAOYSA-N
SMILES: B1(O)C2=CC([N+]([O-])=O)=CC=C2C(C)(C)O1

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: D480708
Product name: 3,3-Dimethyl-6-Nitrobenzo[C][1,2]Oxaborol-1(3H)-Ol
Packaging: 2.5mg
Price: $45
Updated: 2021/12/16

TRC

Product number: D480708
Product name: 3,3-Dimethyl-6-Nitrobenzo[C][1,2]Oxaborol-1(3H)-Ol
Packaging: 25mg
Price: $175
Updated: 2021/12/16

Crysdot

Product number: CD11303613
Product name: 3,3-Dimethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol
Purity: 95+%
Packaging: 1g
Price: $892
Updated: 2021/12/16

Crysdot

Product number: CD11303613
Product name: 3,3-Dimethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol
Purity: 95+%
Packaging: 5g
Price: $2679
Updated: 2021/12/16

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3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol Chemical Properties,Usage,Production

Chemical Properties

Yellow solid

Synthesis

At -40°C, to 100% fuming nitric acid (10 mL) was added dropwise a solution of 3,3-dimethylbenzo[c][l,2]oxaborol-l(3H)-ol (XCVI) (1.37 g, 0.0085 mol) in carbon tetrachloride (40 mL), maintaining the temperature below -40°C. After 20 min, the yellow solution was poured into ice and was stirred for 10 min at RT. The mixture was extracted with EtOAc. 1M aqueous NaOH was added to the organic layer to adjust the pH=7. The organic layer was separated, and washed with water, dried over MgS04, and filtered, and the solvent was removed in vacuo to give an orange viscous oil. The oily residue was triturated with hexane to give pure 3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol.

3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol Preparation Products And Raw materials

Raw materials

Preparation Products

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3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol Suppliers

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1266084-47-2, 3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-olRelated Search:

3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol

1,3-dihydro-1-hydroxy-3,3-dimethyl-6-nitro-2,1-Benzoxaborole

3,3-Dimethyl-6-Nitrobenzo[C][1,2]Oxaborol-1(3H)-Ol(WXC00403)

2,1-Benzoxaborole, 1,3-dihydro-1-hydroxy-3,3-dimethyl-6-nitro-

1266084-47-2