2-nitro-4-bromo-5-fluoroanisole

Product Name: 2-nitro-4-bromo-5-fluoroanisole
CAS No.: 1352244-77-9
Chemical Name: 2-nitro-4-bromo-5-fluoroanisole
Synonyms: 2-nitro-4-bromo-5-fluoroanisole;4-Bromo-5-fluoro-2-nitroanisole;2-Nitro-4-Bromo-5-fluorobenzyl ether;1-bromo-2-fluoro-4-methoxy-5-nitrobenzene;Benzene, 1-bromo-2-fluoro-4-methoxy-5-nitro-
CBNumber: CB32745157
Molecular Formula: C7H5BrFNO3
Formula Weight: 250.02
MOL File: 1352244-77-9.mol

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2-nitro-4-bromo-5-fluoroanisole Property

Boiling point:: 290.5±35.0 °C(Predicted)
Density: 1.716±0.06 g/cm3(Predicted)
storage temp.: 2-8°C
Appearance: White to yellow Solid
InChI: InChI=1S/C7H5BrFNO3/c1-13-7-3-5(9)4(8)2-6(7)10(11)12/h2-3H,1H3
InChIKey: DHSGXAGGBXJPEL-UHFFFAOYSA-N
SMILES: C1(Br)=CC([N+]([O-])=O)=C(OC)C=C1F

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B692458
Product name: 1-Bromo-2-fluoro-4-methoxy-5-nitrobenzene
Packaging: 250mg
Price: $305
Updated: 2021/12/16

AK Scientific

Product number: 8482DK
Product name: 1-Bromo-2-fluoro-4-methoxy-5-nitrobenzene
Packaging: 100mg
Price: $136
Updated: 2021/12/16

AK Scientific

Product number: CS-0041445
Product name: 1-Bromo-2-fluoro-4-methoxy-5-nitrobenzene
Packaging: 1g
Price: $274
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0065043
Product name: 1-BROMO-2-FLUORO-4-METHOXY-5-NITROBENZENE
Purity: 95.00%
Packaging: 5MG
Price: $501.2
Updated: 2021/12/16

Ambeed

Product number: A121679
Product name: 1-Bromo-2-fluoro-4-methoxy-5-nitrobenzene
Purity: 97%
Packaging: 100mg
Price: $32
Updated: 2021/12/16

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2-nitro-4-bromo-5-fluoroanisole Chemical Properties,Usage,Production

Synthesis

458-50-4

1352244-77-9

General procedure for the synthesis of 1-bromo-2-fluoro-4-methoxy-5-nitrobenzene from 4-bromo-3-fluoroanisole: To a solution of 1-bromo-2-fluoro-4-methoxybenzene (5.00 g, 24.39 mmol) in sulphuric acid (20.0 mL) was added potassium nitrate (2.47 g, 24.39 mmol) in batches at 0 °C. The reaction mixture was stirred continuously at 0°C for 0.5 hr. The progress of the reaction was monitored by thin layer chromatography (TLC, unfolding agent ratio of petroleum ether: ethyl acetate = 3:1) to confirm the completion of the reaction. The reaction mixture was quenched by slowly pouring into ice water (50.0 mL) and extracted with ethyl acetate (100 mL x 2). The organic layers were combined, dried with anhydrous sodium sulfate, filtered and concentrated to dryness under reduced pressure to afford 1-bromo-2-fluoro-4-methoxy-5-nitrobenzene (5.55 g, 90% yield) as a white solid.

References

[1] Patent: CN105330698, 2016, A. Location in patent: Paragraph 0566; 0567; 0568; 0569

2-nitro-4-bromo-5-fluoroanisole Preparation Products And Raw materials

Raw materials

Preparation Products

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2-nitro-4-bromo-5-fluoroanisole Suppliers

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View Lastest Price from 2-nitro-4-bromo-5-fluoroanisole manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: 2-nitro-4-bromo-5-fluoroanisole 1352244-77-9
Price: US $2.00-6.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 100kg
Release date: 2025-08-06

Qingdao RENAS Polymer Material Co., Ltd.

Product: 1-bromo-2-fluoro-4-methoxy-5-nitrobenzene 1352244-77-9
Price: US $0.00/kg
Min. Order: 20kg
Purity: 99%
Supply Ability: 20 tons
Release date: 2025-04-25

Shaanxi Dideu New Materials Co. Ltd

Product: 2-nitro-4-bromo-5-fluoroanisole 1352244-77-9
Price: US $0.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 10000KGS
Release date: 2025-03-10

1352244-77-9, 2-nitro-4-bromo-5-fluoroanisoleRelated Search:

2-nitro-4-bromo-5-fluoroanisole

1-bromo-2-fluoro-4-methoxy-5-nitrobenzene

4-Bromo-5-fluoro-2-nitroanisole

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2-Nitro-4-Bromo-5-fluorobenzyl ether

1352244-77-9