ChemicalBook > CAS DataBase List > 2,5-DICHLORO-P-XYLENE

2,5-DICHLORO-P-XYLENE

Product Name
2,5-DICHLORO-P-XYLENE
CAS No.
1124-05-6
Chemical Name
2,5-DICHLORO-P-XYLENE
Synonyms
,5-DICHLORO-P-XYLENE;2,5-DICHLORO-P-XYLENE;1,4-Dichloro-p-xylene;p-xylene,2,5-dichloro-;p-Xylene, 2,5-dichloro-;2,5-Dichloro-para-xylene;2,5-two chloroparaxylene;2,5-Dichloro-p-xylene 97%;2,5-Dichloro-p-xylene >2,5-DICHLORO-P-XYLENE 98+%
CBNumber
CB3281237
Molecular Formula
C8H8Cl2
Formula Weight
175.06
MOL File
1124-05-6.mol
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2,5-DICHLORO-P-XYLENE Property

Melting point:
69-70 °C (lit.)
Boiling point:
222 °C (lit.)
Density 
1.2520 (estimate)
refractive index 
1.5544 (estimate)
Flash point:
221-223°C
storage temp. 
Sealed in dry,Room Temperature
solubility 
Chloroform (Sparingly), DMSO (Slightly, Heated), Hexanes (Slightly), Methanol
form 
Solid
color 
White to Pale Yellow
InChIKey
UTGSRNVBAFCOEU-UHFFFAOYSA-N
CAS DataBase Reference
1124-05-6(CAS DataBase Reference)
NIST Chemistry Reference
Benzene, 1,4-dichloro-2,5-dimethyl-(1124-05-6)
EPA Substance Registry System
2,5-Dichloro-p-xylene (1124-05-6)
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Safety

Risk Statements 
36/37/38
Safety Statements 
26-37
WGK Germany 
3
TSCA 
Yes
HS Code 
2903.99.8001
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
D76404
Product name
2,5-Dichloro-p-xylene
Purity
97%
Packaging
25g
Price
$85.4
Updated
2023/01/07
Sigma-Aldrich
Product number
D76404
Product name
2,5-Dichloro-p-xylene
Purity
97%
Packaging
100g
Price
$193
Updated
2023/01/07
TCI Chemical
Product number
D0431
Product name
2,5-Dichloro-p-xylene
Packaging
25G
Price
$88
Updated
2025/07/31
TRC
Product number
D438885
Product name
2,5-Dichloro-1,4-dimethylbenzene
Packaging
1g
Price
$50
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD64667
Product name
2,5-Dichloro-1,4-dimethylbenzene
Packaging
50g
Price
$50
Updated
2021/12/16
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2,5-DICHLORO-P-XYLENE Chemical Properties,Usage,Production

Uses

2,5-Dichloro-1,4-dimethylbenzene can be used to produce phototropic photosensitive composition containing fluoran colorformer.

Synthesis

106-42-3

1124-05-6

The general procedure for the synthesis of 2,5-dichloro-p-xylene from p-xylene is as follows: In a 500 ml round-bottomed flask, 330 grams of p-xylene (3.1 moles), 0.50 grams (0.003 moles) of ferric chloride, and 0.58 grams (0.003 moles) of dibenzyl sulphide were added and mixed with stirring. The temperature of the mixture was raised to 30°C and 521 g of chlorine gas was slowly passed through the mixture at this temperature over a period of 8 hours. The temperature was gradually raised to about 60°C depending on the cure of the reaction mixture. Upon completion of the chlorination reaction, the crude product was analyzed by gas chromatography, which showed the following composition: degree of chlorination (number of moles of chlorine substituted for 1 mole of p-xylene) 2.21, 2,5-dichloro-p-xylene (2,5-DCPX) 74.5%, 2,3-dichloro-p-xylene (2,3-DCPX) 5.1%, trichloro-p-xylene 19.9%, tetrachloro-p-xylene 0.5%. Subsequently, the crude product was purged with nitrogen and distilled according to the same method as in Example 1 to obtain 255.6 g of crude 2,5-DCPX with a purity of 93.9%. 281.8 g of isopropanol was added thereto, heated to 60° C. to dissolve the crystals, and cooled to 19° C. to crystallize, to ultimately obtain 187 g (53.4% yield) of 2,5-DCPX with a 99.9% purity .

References

[1] Patent: JP2017/190306, 2017, A. Location in patent: Paragraph 0024
[2] Helvetica Chimica Acta, 1944, vol. 27, p. 274,290
[3] Patent: US2412389, 1943,
[4] Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1935, vol. 200, p. 936
[5] Annales de Chimie (Cachan, France), 1936, vol. <11> 5, p. 5,57

2,5-DICHLORO-P-XYLENE Preparation Products And Raw materials

Raw materials

Preparation Products

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2,5-DICHLORO-P-XYLENE Suppliers

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View Lastest Price from 2,5-DICHLORO-P-XYLENE manufacturers

Hebei Chuanghai Biotechnology Co., Ltd
Product
2,5-DICHLORO-P-XYLENE 1124-05-6
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20 mt
Release date
2024-11-18
Hebei Chuanghai Biotechnology Co,.LTD
Product
2,5-DICHLORO-P-XYLENE 1124-05-6
Price
US $5.00-2.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10000kg
Release date
2024-08-22
Henan Fengda Chemical Co., Ltd
Product
2,5-DICHLORO-P-XYLENE 1124-05-6
Price
US $100.00-1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2023-12-26

1124-05-6, 2,5-DICHLORO-P-XYLENERelated Search:


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  • 2,5-DICHLORO-P-XYLENE 98+%
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