5-FLUOROBENZENE-1,3-DIOL

Product Name: 5-FLUOROBENZENE-1,3-DIOL
CAS No.: 75996-29-1
Chemical Name: 5-FLUOROBENZENE-1,3-DIOL
Synonyms: 5-Fluororesorcinol;1,3-Benzenediol, 5-fluoro-
CBNumber: CB33040831
Molecular Formula: C6H5FO2
Formula Weight: 128.1
MOL File: 75996-29-1.mol

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5-FLUOROBENZENE-1,3-DIOL Property

Melting point:: 136.0 to 140.0 °C
Boiling point:: 237.9±10.0 °C(Predicted)
Density: 1.415±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
Water Solubility: Practically insoluble in water
form: powder to crystal
pka: 8.45±0.10(Predicted)
color: White to Light yellow to Light orange

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Safety

HS Code: 2908190090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TCI Chemical

Product number: F1081
Product name: 5-Fluororesorcinol
Purity: >98.0%(GC)(T)
Packaging: 200mg
Price: $320
Updated: 2026/03/19

TCI Chemical

Product number: F1081
Product name: 5-Fluororesorcinol
Purity: >98.0%(GC)(T)
Packaging: 1g
Price: $963
Updated: 2026/03/19

TRC

Product number: F598208
Product name: 5-Fluorobenzene-1,3-diol
Packaging: 50mg
Price: $155
Updated: 2021/12/16

Apolloscientific

Product number: PC910226
Product name: 5-Fluorobenzene-1,3-diol
Purity: 95%
Packaging: 1g
Price: $330
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0355081
Product name: 5-FLUORO-BENZENE-1,3-DIOL
Purity: 95.00%
Packaging: 5MG
Price: $496.5
Updated: 2021/12/16

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5-FLUOROBENZENE-1,3-DIOL Chemical Properties,Usage,Production

Synthesis

52189-63-6

75996-29-1

General procedure for the synthesis of 5-fluororesorcinol from 1,3-dimethoxy-5-fluorobenzene: 1,3-dimethoxy-5-fluorobenzene (10 g, 64 mmol) was dissolved in anhydrous dichloromethane (40 mL) and the solution was cooled to -30 °C. A solution of BBr3 (35.93 mL, 384 mmol) in 60 mL of dichloromethane was added slowly and dropwise to the cooled solution over 30 minutes. After the dropwise addition, the reaction mixture was slowly warmed to 25 °C and stirred continuously for 12 hours. The reaction process was monitored by thin layer chromatography (TLC) using 30% ethyl acetate and petroleum ether as elution solvents. Upon completion of the reaction, the mixture was cooled to 0 °C and quenched by the slow addition of water, followed by stirring at 25 °C for 30 min. The reaction mixture was extracted with dichloromethane (3 x 100 mL), and the combined organic layers were washed with sodium bicarbonate solution, dried over anhydrous sodium sulfate, and concentrated to give 5-fluororesorcinol (2) as a light brown solid. Yield: 8 g (97%).

References

[1] Patent: WO2013/90921, 2013, A1. Location in patent: Paragraph 00154
[2] Patent: WO2014/153000, 2014, A1. Location in patent: Paragraph 0321
[3] Patent: US2016/60260, 2016, A1. Location in patent: Paragraph 0237
[4] Journal of Organic Chemistry, 1997, vol. 62, # 19, p. 6469 - 6475
[5] Journal of Materials Chemistry, 2002, vol. 12, # 5, p. 1316 - 1324

5-FLUOROBENZENE-1,3-DIOL Preparation Products And Raw materials

Raw materials

Preparation Products

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5-FLUOROBENZENE-1,3-DIOL Suppliers

Americas 1 China 59 Europe 1 India 1 Japan 1 United States 6 Global 69

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75996-29-1, 5-FLUOROBENZENE-1,3-DIOLRelated Search:

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75996-29-1

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