ChemicalBook > CAS DataBase List > 6-Methylquinolin-8-ol
6-Methylquinolin-8-ol
- Product Name
- 6-Methylquinolin-8-ol
- CAS No.
- 20984-33-2
- Chemical Name
- 6-Methylquinolin-8-ol
- Synonyms
- 6-Methylquinolin-8-ol;8-Quinolinol, 6-methyl-;6-Methyl-8-hydroxyquinoline
- CBNumber
- CB33065731
- Molecular Formula
- C10H9NO
- Formula Weight
- 159.18
- MOL File
- 20984-33-2.mol
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6-Methylquinolin-8-ol Property
- Melting point:
- 95.5°C
- Boiling point:
- 284.68°C (rough estimate)
- Density
- 1.1202 (rough estimate)
- refractive index
- 1.6070 (estimate)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- Appearance
- Yellow to brown Solid
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
AK Scientific
- Product number
- 4383CA
- Product name
- 6-Methylquinolin-8-ol
- Packaging
- 1g
- Price
- $566
- Updated
- 2021/12/16
Ambeed
- Product number
- A249584
- Product name
- 6-Methylquinolin-8-ol
- Purity
- 98%
- Packaging
- 100mg
- Price
- $94
- Updated
- 2021/12/16
Ambeed
- Product number
- A249584
- Product name
- 6-Methylquinolin-8-ol
- Purity
- 98%
- Packaging
- 250mg
- Price
- $157
- Updated
- 2021/12/16
Alichem
- Product number
- 20984332
- Product name
- 8-Hydroxy-6-methylquinoline
- Packaging
- 250mg
- Price
- $195.75
- Updated
- 2021/12/16
Crysdot
- Product number
- CD11167107
- Product name
- 6-Methylquinolin-8-ol
- Purity
- 98%
- Packaging
- 1g
- Price
- $356
- Updated
- 2021/12/16
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6-Methylquinolin-8-ol Chemical Properties,Usage,Production
Synthesis
3054-95-3
2835-98-5
20984-33-2
GENERAL PROCEDURE: A 1N HCl solution (82.5 mL) was added to a round-bottomed flask containing 6-amino-m-cresol (~1 mmol). Acrolein diethyl acetal (2.5 mmol) was then added. The reaction mixture was refluxed at 111 °C for 24 hours. After completion of the reaction, it was cooled to room temperature and neutralized to pH 7-8 with solid Na2CO3. The product was extracted with dichloromethane (3 x 100 mL), the organic layers were combined, dried with anhydrous Na2SO4 and concentrated under reduced pressure. The crude product was purified by column chromatography with the eluent being a mixed solvent of hexane/ethyl acetate or 15% ethyl acetate/cyclohexane with methanol to give the target compound 6-methylquinolin-8-ol.
References
[1] Tetrahedron Letters, 2015, vol. 56, # 46, p. 6436 - 6439
6-Methylquinolin-8-ol Preparation Products And Raw materials
Raw materials
Preparation Products
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