4-CYCLOPROPYLPHENOL
- Product Name
- 4-CYCLOPROPYLPHENOL
- CAS No.
- 10292-61-2
- Chemical Name
- 4-CYCLOPROPYLPHENOL
- Synonyms
- AKOS BAR-1183;4-CYCLOPROPYLPHENOL;Phenol, 4-cyclopropyl-;Phenol, p-cyclopropyl-;4-Cyclopropylphenol98%;4-Cyclopropylphenol 98%;(4-Hydroxyphenyl)cyclopropane
- CBNumber
- CB3321405
- Molecular Formula
- C9H10O
- Formula Weight
- 134.18
- MOL File
- 10292-61-2.mol
4-CYCLOPROPYLPHENOL Property
- Melting point:
- 57-58℃
- Boiling point:
- 248.2±19.0℃ (760 Torr)
- Density
- 1.158±0.06 g/cm3 (20 ºC 760 Torr)
- refractive index
- 1.5618 (589.3 nm 20℃)
- Flash point:
- 119.8±11.0℃
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 10.05±0.13(Predicted)
- Appearance
- Off-white to yellow Solid
Safety
- HS Code
- 2907199090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H303May be harmfulif swallowed
H314Causes severe skin burns and eye damage
H371May cause damage to organs
H373May cause damage to organs through prolonged or repeated exposure
H411Toxic to aquatic life with long lasting effects
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P273Avoid release to the environment.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P363Wash contaminated clothing before reuse.
P391Collect spillage. Hazardous to the aquatic environment
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- C992445
- Product name
- 4-Cyclopropylphenol
- Packaging
- 25mg
- Price
- $110
- Updated
- 2021/12/16
- Product number
- CHM0389935
- Product name
- 4-CYCLOPROPYLPHENOL
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $502.23
- Updated
- 2021/12/16
- Product number
- Z3817
- Product name
- 4-Cyclopropylphenol
- Packaging
- 5g
- Price
- $616
- Updated
- 2021/12/16
- Product number
- 35518
- Product name
- 4-Cyclopropylphenol
- Purity
- 95+%
- Packaging
- 1g
- Price
- $650
- Updated
- 2021/12/16
- Product number
- OR70008
- Product name
- 4-Cyclopropylphenol
- Packaging
- 250mg
- Price
- $68
- Updated
- 2021/12/16
4-CYCLOPROPYLPHENOL Chemical Properties,Usage,Production
Synthesis
75-11-6
2628-16-2
10292-61-2
To a solution of diethylzinc (59 mL, 65.9 mmol) in toluene (80 mL) was sequentially added 4-acetoxystyrene (5 mL, 32.7 mmol) and diiodomethane (6.86 mL, 85 mmol). The reaction mixture was stirred at room temperature for 5 hours and then heated to reflux for 12 hours. Upon completion of the reaction, the reaction was quenched with 2N HCl solution, the organic layer was separated, washed with brine, dried over anhydrous Na2SO4, and concentrated under reduced pressure to give a brown oily crude product (4.5 g). The crude product was dissolved in methanol/tetrahydrofuran (20 mL/20 mL) mixed solvent, sodium carbonate (5.41 g, 51.1 mmol) was added, and stirred at room temperature for 2 hours. The reaction mixture was diluted with ethyl acetate and washed sequentially with saturated aqueous ammonium chloride solution and water, and the aqueous phase was back-extracted with ethyl acetate (3×). The organic phases were combined, dried over anhydrous Na2SO4 and concentrated under reduced pressure to afford 4-cyclopropylphenol (3.2 g, 94% yield), the product could be used for subsequent reactions without further purification.
References
[1] Patent: US2011/105520, 2011, A1. Location in patent: Page/Page column 55
4-CYCLOPROPYLPHENOL Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-CYCLOPROPYLPHENOL manufacturers
- Product
- 4-CYCLOPROPYLPHENOL 10292-61-2
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-11
- Product
- 4-CYCLOPROPYLPHENOL 10292-61-2
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-09
- Product
- 4-CYCLOPROPYLPHENOL 10292-61-2
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 10000KGS
- Release date
- 2020-01-11