ChemicalBook > CAS DataBase List > 1,10-Dibromodecane

1,10-Dibromodecane

Product Name
1,10-Dibromodecane
CAS No.
4101-68-2
Chemical Name
1,10-Dibromodecane
Synonyms
,w-Dibromodecane;Dibromodecane,95%;1,10-DIBROMODECANE;1,10-dibromo-decan;TIMTEC-BB SBB008900;Decene, 1,10-dibromo;Decane, 1,10-dibromo-;1,10-DECANE DIBROMIDE;DECAMETHYLENE BROMIDE;1,10-Dibromodecane,97%
CBNumber
CB3322169
Molecular Formula
C10H20Br2
Formula Weight
300.07
MOL File
4101-68-2.mol
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1,10-Dibromodecane Property

Melting point:
25-27 °C (lit.)
Boiling point:
160 °C/15 mmHg (lit.)
Density 
1.335 g/mL at 25 °C (lit.)
refractive index 
n20/D 1.4912(lit.)
Flash point:
26°C
storage temp. 
Sealed in dry,Room Temperature
form 
Crystalline Low Melting Solid
Specific Gravity
1.335
color 
Beige to brown
Water Solubility 
insoluble
BRN 
506156
Dielectric constant
6.5599999999999996
InChIKey
GTQHJCOHNAFHRE-UHFFFAOYSA-N
CAS DataBase Reference
4101-68-2(CAS DataBase Reference)
NIST Chemistry Reference
Decane, 1,10-dibromo-(4101-68-2)
EPA Substance Registry System
Decane, 1,10-dibromo- (4101-68-2)
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Safety

Hazard Codes 
C,Xi
Risk Statements 
20/21/22-36/37/38
Safety Statements 
22-24/25-36-26
WGK Germany 
3
TSCA 
Yes
HS Code 
29049090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
D39800
Product name
1,10-Dibromodecane
Purity
97%
Packaging
100g
Price
$124
Updated
2025/07/31
TCI Chemical
Product number
D0179
Product name
1,10-Dibromodecane
Purity
>95.0%(GC)
Packaging
25g
Price
$30
Updated
2025/07/31
TCI Chemical
Product number
D0179
Product name
1,10-Dibromodecane
Purity
>95.0%(GC)
Packaging
100g
Price
$104
Updated
2025/07/31
TRC
Product number
D448868
Product name
1,10-Dibromodecane
Packaging
10g
Price
$75
Updated
2021/12/16
TRC
Product number
D448868
Product name
1,10-Dibromodecane
Packaging
1g
Price
$45
Updated
2021/12/16
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1,10-Dibromodecane Chemical Properties,Usage,Production

Chemical Properties

beige to brown crystalline low melting mass

Uses

1,10-Dibromodecane is used as an alkylating agent and as synthetic organic intermediate.

Synthesis

112-47-0

4101-68-2

The general procedure for the synthesis of 1,10-dibromodecane from 1,10-decanediol is as follows: 1,10-decanediol (1 eq.), 48% aqueous hydrobromic acid (ca. 3 eq./hydroxyl), and octane (ca. 7:1 volume-to-weight ratio to the diol) were added to a single-necked, round-bottomed flask and assembled with a fractionating column/Dean-Stark trap. The reaction mixture was placed in a heated oil bath (145-150°C) with rapid magnetic stirring. The aqueous (lower) layer at the initial boiling point (89-92°C) was condensed and gently separated, and subsequently collected at about half the theoretical volume of water; at this point the temperature of the azeotrope (still at head temperature) began to rise. The condenser was set to full reflux for a few hours, then turned back on and the aqueous-phase material continued to be collected for 1 hour (top temperature 96-100°C). The final volume of the aqueous phase distillate reaches 90-100% of the theoretical value (up to 24% hydrobromic acid in the high boiling distillate). When the octane phase (which is light tan in color) contains dibromides and brominated streptanols (e.g., 6 band 6c), it is washed with cold 85% v/v sulfuric acid (10 mL first, then 5 mL) to remove all color and brominated streptanols. For all three dibromides (3b, 4b, 6b), the neutralized octane solution was passed through a Vigreux column under reduced pressure to remove the solvent, and the residue (which was confirmed to be essentially pure by 1H NMR) was purified by Kugelrohr distillation. Trace amounts of 4-methyltetrahydropyran were detected prior to distillation of 4b.

References

[1] Tetrahedron Letters, 2015, vol. 56, # 4, p. 630 - 632
[2] Green Chemistry, 2014, vol. 16, # 2, p. 836 - 843
[3] Journal of Organic Chemistry, 2015, vol. 80, # 11, p. 5386 - 5394
[4] Journal of the American Chemical Society, 1936, vol. 58, p. 488
[5] Journal of the Chemical Society, 1958, p. 2068

1,10-Dibromodecane Preparation Products And Raw materials

Raw materials

Hydrogen bromide DECYLENE GLYCOL

Preparation Products

12-MERCAPTODODECANOIC ACID
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1,10-Dibromodecane Suppliers

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View Lastest Price from 1,10-Dibromodecane manufacturers

Hebei Chuanghai Biotechnology Co., Ltd
Product
1,10-Dibromodecane 4101-68-2
Price
US $0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
500000kg
Release date
2024-10-25
Henan Aochuang Chemical Co.,Ltd.
Product
1,10-Dibromodecane 4101-68-2
Price
US $0.00-0.00/kg
Min. Order
1kg
Purity
98%
Supply Ability
1Ton
Release date
2022-09-26
Hebei Yanxi Chemical Co., Ltd.
Product
1,10-Dibromodecane 4101-68-2
Price
US $0.00/kg
Min. Order
1kg
Purity
0.985
Supply Ability
20tons
Release date
2023-10-13

4101-68-2, 1,10-DibromodecaneRelated Search:

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