ChemicalBook > CAS DataBase List > 2-AMINO-1H-BENZIMIDAZOLE-5-CARBOXYLIC ACID

2-AMINO-1H-BENZIMIDAZOLE-5-CARBOXYLIC ACID

Product Name: 2-AMINO-1H-BENZIMIDAZOLE-5-CARBOXYLIC ACID
CAS No.: 76391-97-4
Chemical Name: 2-AMINO-1H-BENZIMIDAZOLE-5-CARBOXYLIC ACID
Synonyms: 2-AMINO-BENZIMIDAZOLE-5-CARBOXYLIC ACID;2-AMINO-1H-BENZIMIDAZOLE-5-CARBOXYLIC ACID;2-amino-1H-Benzimidazole-6-carboxylic acid;2-amino-3h-benzimidazole-5-carboxylic Acid;2-AMINO-1H-BENZOIMIDAZOLE-5-CARBOXYLIC ACID;1H-Benzimidazole-6-carboxylicacid, 2-amino-;2-amino-1H-benzo[d]imidazole-5-carboxylic acid;1H-Benzimidazole-5-carboxylicacid,2-amino-(9CI);2-Amino-1H-benzimidazole-5-carboxylic acid, CAS 76391-97-4
CBNumber: CB3322932
Molecular Formula: C8H7N3O2
Formula Weight: 177.16
MOL File: 76391-97-4.mol

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2-AMINO-1H-BENZIMIDAZOLE-5-CARBOXYLIC ACID Property

Boiling point:: 540.4±42.0 °C(Predicted)
Density: 1.611±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
pka: 3.17±0.30(Predicted)
Appearance: Light brown to brown Solid

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Safety

Hazard Codes: Xi
Risk Statements: 36
Safety Statements: 26

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

Biosynth Carbosynth

Product number: FA151544
Product name: 2-Amino-1H-benzimidazole-5-carboxylicacid
Packaging: 10mg
Price: $100
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA151544
Product name: 2-Amino-1H-benzimidazole-5-carboxylicacid
Packaging: 25mg
Price: $150
Updated: 2021/12/16

ChemScene

Product number: CS-0060644
Product name: 2-Amino-1H-benzo[d]imidazole-5-carboxylicacid
Packaging: 100mg
Price: $190
Updated: 2021/12/16

AK Scientific

Product number: 9383AJ
Product name: 2-Amino-1H-benzimidazole-5-carboxylicacid
Packaging: 250mg
Price: $239
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA151544
Product name: 2-Amino-1H-benzimidazole-5-carboxylicacid
Packaging: 50mg
Price: $250
Updated: 2021/12/16

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2-AMINO-1H-BENZIMIDAZOLE-5-CARBOXYLIC ACID Chemical Properties,Usage,Production

Synthesis

506-68-3

36692-49-6

76391-97-4

1. Cyanogen bromide solution (5.0 mL, 5 M in acetonitrile, 25 mmol) was slowly added to a suspension in water (50 mL) containing methyl 3,4-diaminobenzoate (3.0 g, 18 mmol). 2. The reaction mixture was stirred overnight at room temperature. 3. Upon completion of the reaction, ammonia (20 mL) and ethyl acetate (100 mL) were added to the mixture and mixed thoroughly to separate the organic and aqueous layers. 4. The organic layer was dried with anhydrous sodium sulfate, filtered to remove the desiccant, and the organic phase was subsequently concentrated under reduced pressure. 5. 2 N aqueous hydrochloric acid (18 mL, 36.0 mmol) was added to the concentrated crude product and the mixture was heated to reflux and the reaction continued overnight. 6. At the end of the reaction, the reaction mixture was concentrated under reduced pressure to afford 2-amino-1H-benzo[d]imidazole-5-carboxylic acid (2.90 g, 97% yield). 7. The structure of the product was confirmed by 1H NMR (400 MHz, DMSO-d6): δ 8.75 (s, 2H), 7.84 (s, 1H), 7.77 (dd, J = 1.2, 8.4 Hz, 1H), 7.38 (d, J = 8.4 Hz, 1H).

References

[1] Patent: US2012/108619, 2012, A1. Location in patent: Page/Page column 39
[2] Patent: US2012/270893, 2012, A1. Location in patent: Page/Page column 27

2-AMINO-1H-BENZIMIDAZOLE-5-CARBOXYLIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-AMINO-1H-BENZIMIDAZOLE-5-CARBOXYLIC ACID manufacturers

Career Henan Chemical Co

Product: 2-AMINO-1H-BENZIMIDAZOLE-5-CARBOXYLIC ACID 76391-97-4
Price: US $3.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 200KG
Release date: 2020-03-26

76391-97-4, 2-AMINO-1H-BENZIMIDAZOLE-5-CARBOXYLIC ACIDRelated Search:

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2-Amino-1H-benzimidazole-5-carboxylic acid, CAS 76391-97-4

76391-97-4

BENZIMIDAZOLE