3-HYDROXY-4-METHYL-BENZALDEHYDE

Product Name: 3-HYDROXY-4-METHYL-BENZALDEHYDE
CAS No.: 57295-30-4
Chemical Name: 3-HYDROXY-4-METHYL-BENZALDEHYDE
Synonyms: 3-hydroxy-4-methybenzaldehyde;3-hydroxy-4-methyl-benaldehyde;3-HYDROXY-4-METHYL-BENZALDEHYDE;Benzaldehyde, 3-hydroxy-4-Methyl-;N-[2-(dimethylamino)ethyl]-2-methylbenzamide
CBNumber: CB3326703
Molecular Formula: C8H8O2
Formula Weight: 136.15
MOL File: 57295-30-4.mol

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3-HYDROXY-4-METHYL-BENZALDEHYDE Property

Melting point:: 73-74 °C
Boiling point:: 252.4±20.0 °C(Predicted)
Density: 1.175±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 9.59±0.10(Predicted)
Appearance: Off-white to yellow Solid
InChI: InChI=1S/C8H8O2/c1-6-2-3-7(5-9)4-8(6)10/h2-5,10H,1H3
InChIKey: DHVJHJQBQKKPNB-UHFFFAOYSA-N
SMILES: C(=O)C1=CC=C(C)C(O)=C1

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Safety

Hazard Codes: Xi
Risk Statements: 41
Safety Statements: 26-39
HS Code: 2912490090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: H517775
Product name: 3-Hydroxy-4-methylbenzaldehyde
Packaging: 500mg
Price: $175
Updated: 2021/12/16

Apolloscientific

Product number: OR942429
Product name: 3-Hydroxy-4-methyl-benzaldehyde
Purity: 95%
Packaging: 250mg
Price: $247
Updated: 2021/12/16

Apolloscientific

Product number: OR942429
Product name: 3-Hydroxy-4-methyl-benzaldehyde
Purity: 95%
Packaging: 1g
Price: $609
Updated: 2021/12/16

AK Scientific

Product number: Z0696
Product name: 3-Hydroxy-4-methyl-benzaldehyde
Packaging: 250mg
Price: $131
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0165763
Product name: 3-HYDROXY-4-METHYL-BENZALDEHYDE
Purity: 98.00%
Packaging: 5G
Price: $2021.25
Updated: 2021/12/16

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3-HYDROXY-4-METHYL-BENZALDEHYDE Chemical Properties,Usage,Production

Synthesis

90953-62-1

57295-30-4

General procedure for the synthesis of compounds (CAS:57295-30-4) from 5-(hydroxymethyl)-2-methylphenol: The product of step (i) (440.0 mg, 3.18 mmol) was dissolved in THF (4.4 mL) at room temperature, followed by addition of MnO2 (552.9 mg, 6.36 mmol). The reaction mixture was stirred at 50 °C for 6 hours. Upon completion of the reaction, the mixture was filtered through a diatomaceous earth pad to remove solid impurities. The filtrate was concentrated and the residue was purified by fast column chromatography to afford the target compound (CAS:57295-30-4) (46.1 mg, 11% yield) as a light yellow solid.1H NMR (CDCl3) δ: 9.90 (1H, s), 7.36 (1H, dd, J = 7.76, 1.44 Hz), 7.30 (1H, s ), 7.29 (1H, d, J = 5.52 Hz), 5.33 (1H, s), 2.33 (3H, s).

Purification Methods

Crystallise it from water or *C6H6 (m 71-71o). The O-methyl ether has m 45-46o (from Et2O/hexane). [Sedgwick & Allott J Chem Soc 2820 1923, Flitsch et al. Justus Liebigs Ann Chem 1413 1985, Beilstein 8 H 100, 8 II 103, 8 IV 368.]

References

[1] Patent: US2011/136801, 2011, A1. Location in patent: Page/Page column 44

3-HYDROXY-4-METHYL-BENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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3-HYDROXY-4-METHYL-BENZALDEHYDE Suppliers

China 74 India 2 Sweden 1 United Kingdom 6 United States 6 Global 89

Suzhou Heyi Biochemical Technology Co., Ltd.

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Hangzhou J&H Chemical Co., Ltd.

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Shanghai HuanChuan Industry Co.,Ltd.

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Cool Pharm, Ltd

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View Lastest Price from 3-HYDROXY-4-METHYL-BENZALDEHYDE manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: 3-Hydroxy-4-methylbenzaldehyde 57295-30-4
Price: US $3.00-9.00/KG
Min. Order: 0.1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2025-06-19

Career Henan Chemical Co

Product: 3-HYDROXY-4-METHYL-BENZALDEHYDE 57295-30-4
Price: US $1.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 100KG
Release date: 2018-12-16

57295-30-4, 3-HYDROXY-4-METHYL-BENZALDEHYDERelated Search:

Alizarin Complexone 3,5-DIMETHOXY-4-METHYLBENZOIC ACID 3-Methoxy-4-methylbenzoic acid 3-HYDROXY-4-METHYL-2-NITROBENZOIC ACID 3,5-Dihydroxy-4-methylbenzoic acid PSOROMIC ACID 3-Hydroxy-4-methylbenzoic acid GOSSYPOL Rhein Actinomycin D 3-BROMO-2-HYDROXY-5-METHYL-BENZALDEHYDE 5-CHLORO-2-HYDROXY-4-METHYL-BENZALDEHYDE METHYL 3,5-DIMETHOXY-4-METHYLBENZOATE 2,5-DIMETHOXYTEREPHTHALALDEHYDE CATENARIN CYNODONTIN ISLANDICIN SENNIDINE A

3-HYDROXY-4-METHYL-BENZALDEHYDE

Benzaldehyde, 3-hydroxy-4-Methyl-

3-hydroxy-4-methyl-benaldehyde

N-[2-(dimethylamino)ethyl]-2-methylbenzamide

3-hydroxy-4-methybenzaldehyde

57295-30-4

Aromatic Aldehydes & Derivatives (substituted)