4-NITROHOMOPHTHALIC ACID
- Product Name
- 4-NITROHOMOPHTHALIC ACID
- CAS No.
- 3898-66-6
- Chemical Name
- 4-NITROHOMOPHTHALIC ACID
- Synonyms
- Nitrohomophthalic acid;4-NITROHOMOPHTHALIC ACID;4-methoxylhomophthalic acid;2-carboxy-4-nitro-Benzeneacetic acid;2-(CARBOXYMETHYL)-5-NITROBENZOIC ACID;Benzeneacetic acid, 2-carboxy-4-nitro-
- CBNumber
- CB3332667
- Molecular Formula
- C9H7NO6
- Formula Weight
- 225.15
- MOL File
- 3898-66-6.mol
4-NITROHOMOPHTHALIC ACID Property
- Melting point:
- 210-215 °C (decomp)
- Boiling point:
- 484.0±35.0 °C(Predicted)
- Density
- 1.594±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 2.73±0.22(Predicted)
- Appearance
- Light yellow to yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- A178226
- Product name
- 2-(Carboxymethyl)-5-nitrobenzoicacid
- Purity
- 95%
- Packaging
- 100mg
- Price
- $53
- Updated
- 2021/12/16
- Product number
- A178226
- Product name
- 2-(Carboxymethyl)-5-nitrobenzoicacid
- Purity
- 95%
- Packaging
- 250mg
- Price
- $84
- Updated
- 2021/12/16
- Product number
- A178226
- Product name
- 2-(Carboxymethyl)-5-nitrobenzoicacid
- Purity
- 95%
- Packaging
- 1g
- Price
- $211
- Updated
- 2021/12/16
- Product number
- CM252662
- Product name
- 2-(Carboxymethyl)-5-nitrobenzoicacid
- Purity
- 95%
- Packaging
- 1g
- Price
- $299
- Updated
- 2021/12/16
- Product number
- 3898666
- Product name
- 2-(Carboxymethyl)-5-nitrobenzoicacid
- Packaging
- 1g
- Price
- $323.2
- Updated
- 2021/12/16
4-NITROHOMOPHTHALIC ACID Chemical Properties,Usage,Production
Synthesis
89-51-0
3898-66-6
Fuming nitric acid (20 mL) was slowly added dropwise to the homophthalic acid at 0°C. The reaction mixture was then stirred continuously for 5 hours at room temperature. Upon completion of the reaction, the mixture was carefully poured into ice water to quench the reaction. The precipitated solid product was collected by filtration and washed well with cold water. Finally, the product was dried in a desiccator to afford 2-(carboxymethyl)-5-nitrobenzoic acid (2.01 g, 32% yield). The product was analyzed by ESI/APCI(+) mass spectrometry, showing a molecular ion peak m/z of 207.8 ([M+H]+).
References
[1] Journal of Medicinal Chemistry, 2008, vol. 51, # 24, p. 7717 - 7730
[2] Patent: WO2012/85003, 2012, A1. Location in patent: Page/Page column 111-112
[3] Bioorganic and Medicinal Chemistry, 2003, vol. 11, # 14, p. 3141 - 3152
[4] Tetrahedron, 2017, vol. 73, # 7, p. 819 - 828
[5] Journal of Medicinal Chemistry, 2015, vol. 58, # 7, p. 3188 - 3208
4-NITROHOMOPHTHALIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-NITROHOMOPHTHALIC ACID manufacturers
- Product
- 4-NITROHOMOPHTHALIC ACID 3898-66-6
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20T
- Release date
- 2024-08-15