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N3-[1,1'-Biphenyl]-4-yl-N1,N1-diphenyl-1,3-benzenediamine

Product Name
N3-[1,1'-Biphenyl]-4-yl-N1,N1-diphenyl-1,3-benzenediamine
CAS No.
1800322-10-4
Chemical Name
N3-[1,1'-Biphenyl]-4-yl-N1,N1-diphenyl-1,3-benzenediamine
Synonyms
N3-[1,1'-Biphenyl]-4-yl-N1,N1-diphenyl-1,3-benzenediamine;N3-[1,1'-Biphenyl]-4-yl-N1,N1-diphenyl-1,3-benzenediamine;N1-([1,1'-biphenyl]-4-yl)-N3,N3-diphenylbenzene-1,3-diamine;1,3-Benzenediamine, N3-[1,1'-biphenyl]-4-yl-N1,N1-diphenyl-
CBNumber
CB33352880
Molecular Formula
C30H24N2
Formula Weight
412.52
MOL File
1800322-10-4.mol
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Hazard and Precautionary Statements (GHS)

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N3-[1,1'-Biphenyl]-4-yl-N1,N1-diphenyl-1,3-benzenediamine Chemical Properties,Usage,Production

Synthesis


Diphenylamine (37.0 g, 218.64 mmol) was added to a round bottom flask and dissolved in toluene (1100 mL), and 1-bromo-3-chlorobenzene 41.86 g, 218.64 mmol), Pd2(dba)3 (6.01 g, 6.56 mmol), P(t-Bu)3 (2.65 g, 13.12 mmol), NaOt-Bu (63.03 g, 655.9 mmol) were added in the order and stirred at 100 ° C. After the reaction was completed, the reaction mixture was extracted with ether and water. The organic layer was dried over MgSO4 and concentrated. The resultingcompound wasseparated bysilicagelcolumn chromatography andrecrystallized to obtain47.6 g ofthe product. (yield: 78%)

N3-[1,1'-Biphenyl]-4-yl-N1,N1-diphenyl-1,3-benzenediamine Preparation Products And Raw materials

Raw materials

Preparation Products

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1800322-10-4, N3-[1,1'-Biphenyl]-4-yl-N1,N1-diphenyl-1,3-benzenediamineRelated Search:


  • N3-[1,1'-Biphenyl]-4-yl-N1,N1-diphenyl-1,3-benzenediamine
  • 1,3-Benzenediamine, N3-[1,1'-biphenyl]-4-yl-N1,N1-diphenyl-
  • N1-([1,1'-biphenyl]-4-yl)-N3,N3-diphenylbenzene-1,3-diamine
  • N3-[1,1'-Biphenyl]-4-yl-N1,N1-diphenyl-1,3-benzenediamine
  • 1800322-10-4