ChemicalBook > CAS DataBase List > 2-Methoxyethyl 2-[(3-nitrophenyl)methylene]acetoacetate
2-Methoxyethyl 2-[(3-nitrophenyl)methylene]acetoacetate
- Product Name
- 2-Methoxyethyl 2-[(3-nitrophenyl)methylene]acetoacetate
- CAS No.
- 39562-22-6
- Chemical Name
- 2-Methoxyethyl 2-[(3-nitrophenyl)methylene]acetoacetate
- Synonyms
- SALOR-INT L133884-1EA;2-Methoxyethyl 2-[(3-;Nitrendipine Impurity I;UVZJPCAZMGLNTB-UHFFFAOYSA-N;2-Methoxyethyl 2-[(3-nitrophenyl);methoxyethyl 3-nitrobenzylidenacetoacetate;METHOXYRTHYL-3-NITROBENZYLIDENACETOACETATE;(Z)-2-METHOXYETHYL 2-BENZYLIDENE-3-OXOBUTANOATE;2-Methoxyethyl-2-(3-nitrobenzyliden)acetoacetate;2-METHOXYETHYL 2-(3-NITROBENZYLIDENE)ACETOACETATE
- CBNumber
- CB3388558
- Molecular Formula
- C14H15NO6
- Formula Weight
- 293.27
- MOL File
- 39562-22-6.mol
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2-Methoxyethyl 2-[(3-nitrophenyl)methylene]acetoacetate Property
- Melting point:
- 72-74°C
- Boiling point:
- 433.4±40.0 °C(Predicted)
- Density
- 1.266±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,2-8°C
- solubility
- DMSO, Methanol
- form
- Solid
- color
- Off-White to Pale Yellow
- CAS DataBase Reference
- 39562-22-6(CAS DataBase Reference)
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Safety
- HazardClass
- IRRITANT
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H317May cause an allergic skin reaction
H410Very toxic to aquatic life with long lasting effects
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P272Contaminated work clothing should not be allowed out of the workplace.
P273Avoid release to the environment.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P321Specific treatment (see … on this label).
P333+P313IF SKIN irritation or rash occurs: Get medical advice/attention.
P363Wash contaminated clothing before reuse.
P391Collect spillage. Hazardous to the aquatic environment
P501Dispose of contents/container to..…
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N-Bromosuccinimide Price
TRC
- Product number
- M262580
- Product name
- 2-Methoxyethyl2-(3-Nitrobenzylidene)acetoacetate
- Packaging
- 1g
- Price
- $110
- Updated
- 2021/12/16
TRC
- Product number
- M262580
- Product name
- 2-Methoxyethyl2-(3-Nitrobenzylidene)acetoacetate
- Packaging
- 2g
- Price
- $210
- Updated
- 2021/12/16
TRC
- Product number
- M262580
- Product name
- 2-Methoxyethyl2-(3-Nitrobenzylidene)acetoacetate
- Packaging
- 5g
- Price
- $525
- Updated
- 2021/12/16
Frontier Specialty Chemicals
- Product number
- Y15233
- Product name
- 2-Methoxyethyl-2-(3-nitrobenzylidene)acetoacetate
- Purity
- 98%
- Packaging
- 1g
- Price
- $10
- Updated
- 2021/12/16
AK Scientific
- Product number
- P825
- Product name
- Methoxyethyl3-nitrobenzylidenacetoacetate
- Packaging
- 100mg
- Price
- $29
- Updated
- 2021/12/16
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2-Methoxyethyl 2-[(3-nitrophenyl)methylene]acetoacetate Chemical Properties,Usage,Production
Chemical Properties
Off-White to Pale Yellow Solid
Uses
Cilnidipine intermediate.
Hazard
Low toxicity by ingestion and inhalation. A moderate eye irritant.
Synthesis
200 kg of methoxyethyl acetoacetate and 185.1 kg of 3-nitrobenzaldehyde were suspended in 800 l of isopropanol. Then 5.65 kg of p-anisic acid and 5.05 kg of an ethanol solution of 33% dimethylamine were added and heated at about 35??C for about 30 minutes to obtain a solution. The reaction mixture was cooled to 20/25??C, then it was cooled with running water for about 12 hours and cooled with brine at about 0??C for another 24 hours, then centrifuged and washed with isopropanol. After drying, 327 kg of 3-nitrophenylforkylacetoacetic acid methoxyethyl ester was obtained in about 91% yield.
2-Methoxyethyl 2-[(3-nitrophenyl)methylene]acetoacetate Preparation Products And Raw materials
Raw materials
Preparation Products
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2-Methoxyethyl 2-[(3-nitrophenyl)methylene]acetoacetate Suppliers
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View Lastest Price from 2-Methoxyethyl 2-[(3-nitrophenyl)methylene]acetoacetate manufacturers
Hebei Chuanghai Biotechnology Co., Ltd
- Product
- 2-Methoxyethyl 2-[(3-nitrophenyl)methylene]acetoacetate 39562-22-6
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 500000kg
- Release date
- 2024-11-01
Career Henan Chemical Co
- Product
- 2-Methoxyethyl (2E)-2-acetyl-3-(3-nitrophenyl)-acrylate 39562-22-6
- Price
- US $1.00/kg
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2018-12-25
39562-22-6, 2-Methoxyethyl 2-[(3-nitrophenyl)methylene]acetoacetateRelated Search:
Linezolid
Acetic acid
2-(2-Nitrobenzylidene)-3-oxobutanoic Acid, 2-Acetoxy-2-methylpropyl Ester
2-Methoxyethyl acetoacetate
2-Methoxyethyl 2-[(3-nitrophenyl)methylene]acetoacetate
ALPHA-ETHYL-3-NITROCINNAMIC ACID
ETHYL 3-AMINOCINNAMATE
ETHYL 3-NITROCINNAMATE