[2-(1H-PYRROL-1-YL)PHENYL]METHANOL
- Product Name
- [2-(1H-PYRROL-1-YL)PHENYL]METHANOL
- CAS No.
- 61034-86-4
- Chemical Name
- [2-(1H-PYRROL-1-YL)PHENYL]METHANOL
- Synonyms
- (2-pyrrol-1-ylphenyl)methano;2-(Pyrrol-1-yl)benzyl Alcohol;(2-PYRROL-1-YL-PHENYL)-METHANOL;2-(1H-PYRROL-1-YL)BENZYL ALCOHOL;[2-(1H-PYRROL-1-YL)PHENYL]METHANOL;4-Hydroxy-3-Methyl-1H-quinolin-2-one;2-(1H-Pyrrol-1-yl)benzyl alcohol 97%;Benzenemethanol, 2-(1H-pyrrol-1-yl)-;[2-(1H-Pyrrol-1-yl)phenyl]methanol97%;[2-(1H-Pyrrol-1-yl)phenyl]methanol 97%
- CBNumber
- CB3410095
- Molecular Formula
- C11H11NO
- Formula Weight
- 173.21
- MOL File
- 61034-86-4.mol
[2-(1H-PYRROL-1-YL)PHENYL]METHANOL Property
- Melting point:
- 43 °C
- storage temp.
- 2-8°C
Safety
- Hazard Note
- Harmful
- HS Code
- 2906290090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- P998830
- Product name
- (2-(1H-Pyrrol-1-yl)phenyl)methanol
- Packaging
- 1g
- Price
- $175
- Updated
- 2021/12/16
- Product number
- 3H01-1-X0
- Product name
- [2-(1H-Pyrrol-1-yl)phenyl]methanol
- Purity
- 97%
- Packaging
- 250mg
- Price
- $87
- Updated
- 2021/12/16
- Product number
- 3H01-1-X0
- Product name
- [2-(1H-Pyrrol-1-yl)phenyl]methanol
- Purity
- 97%
- Packaging
- 1g
- Price
- $167
- Updated
- 2021/12/16
- Product number
- Y9612
- Product name
- [2-(1H-Pyrrol-1-yl)phenyl]methanol
- Packaging
- 5g
- Price
- $482
- Updated
- 2021/12/16
- Product number
- CHM0016350
- Product name
- [2-(1H-PYRROL-1-YL)PHENYL]METHANOL
- Purity
- 95.00%
- Packaging
- 250MG
- Price
- $656.08
- Updated
- 2021/12/16
[2-(1H-PYRROL-1-YL)PHENYL]METHANOL Chemical Properties,Usage,Production
Synthesis
78540-08-6
61034-86-4
General procedure for the synthesis of 2-(1H-pyrrol-1-yl)benzylethanol from ethyl 2-pyrrol-1-yl-benzoate: ethyl 2-pyrrol-1-yl-benzoate (22.2 g, 103 mmol) was dissolved in toluene (140 mL), stirred and heated to 35 °C. To this solution was slowly added a toluene solution of sodium bis(2-ethoxymethoxy)hydroaluminum (70 wt%, 32 mL, 115 mmol) while maintaining the reaction temperature at 45 °C. After addition, the reaction was continued with stirring at 45°C for 1 hour. Upon completion of the reaction, the mixture was cooled to 0 °C and the reaction was quenched by careful and slow addition of 4N HCl aqueous solution (75 mL). The organic layer was separated, washed with saturated sodium bicarbonate solution (75 mL) and dried over anhydrous magnesium sulfate. The solvent was removed by concentration under reduced pressure to afford the target product 2-(1H-pyrrol-1-yl)benzylethanol (16.8 g, 97 mmol) as a pale yellow oil in 94% yield. Thin layer chromatography (TLC) showed Rf = 0.56 (Expander: dichloromethane/methanol = 97:3).
References
[1] Patent: EP1586559, 2005, A1. Location in patent: Page/Page column 64-65
[2-(1H-PYRROL-1-YL)PHENYL]METHANOL Preparation Products And Raw materials
Raw materials
Preparation Products
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