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[2-(1H-PYRROL-1-YL)PHENYL]METHANOL

Product Name
[2-(1H-PYRROL-1-YL)PHENYL]METHANOL
CAS No.
61034-86-4
Chemical Name
[2-(1H-PYRROL-1-YL)PHENYL]METHANOL
Synonyms
(2-pyrrol-1-ylphenyl)methano;2-(Pyrrol-1-yl)benzyl Alcohol;(2-PYRROL-1-YL-PHENYL)-METHANOL;2-(1H-PYRROL-1-YL)BENZYL ALCOHOL;[2-(1H-PYRROL-1-YL)PHENYL]METHANOL;4-Hydroxy-3-Methyl-1H-quinolin-2-one;2-(1H-Pyrrol-1-yl)benzyl alcohol 97%;Benzenemethanol, 2-(1H-pyrrol-1-yl)-;[2-(1H-Pyrrol-1-yl)phenyl]methanol97%;[2-(1H-Pyrrol-1-yl)phenyl]methanol 97%
CBNumber
CB3410095
Molecular Formula
C11H11NO
Formula Weight
173.21
MOL File
61034-86-4.mol
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[2-(1H-PYRROL-1-YL)PHENYL]METHANOL Property

Melting point:
43 °C
storage temp. 
2-8°C
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Safety

Hazard Note 
Harmful
HS Code 
2906290090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC
Product number
P998830
Product name
(2-(1H-Pyrrol-1-yl)phenyl)methanol
Packaging
1g
Price
$175
Updated
2021/12/16
SynQuest Laboratories
Product number
3H01-1-X0
Product name
[2-(1H-Pyrrol-1-yl)phenyl]methanol
Purity
97%
Packaging
250mg
Price
$87
Updated
2021/12/16
SynQuest Laboratories
Product number
3H01-1-X0
Product name
[2-(1H-Pyrrol-1-yl)phenyl]methanol
Purity
97%
Packaging
1g
Price
$167
Updated
2021/12/16
AK Scientific
Product number
Y9612
Product name
[2-(1H-Pyrrol-1-yl)phenyl]methanol
Packaging
5g
Price
$482
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0016350
Product name
[2-(1H-PYRROL-1-YL)PHENYL]METHANOL
Purity
95.00%
Packaging
250MG
Price
$656.08
Updated
2021/12/16
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[2-(1H-PYRROL-1-YL)PHENYL]METHANOL Chemical Properties,Usage,Production

Synthesis

78540-08-6

61034-86-4

General procedure for the synthesis of 2-(1H-pyrrol-1-yl)benzylethanol from ethyl 2-pyrrol-1-yl-benzoate: ethyl 2-pyrrol-1-yl-benzoate (22.2 g, 103 mmol) was dissolved in toluene (140 mL), stirred and heated to 35 °C. To this solution was slowly added a toluene solution of sodium bis(2-ethoxymethoxy)hydroaluminum (70 wt%, 32 mL, 115 mmol) while maintaining the reaction temperature at 45 °C. After addition, the reaction was continued with stirring at 45°C for 1 hour. Upon completion of the reaction, the mixture was cooled to 0 °C and the reaction was quenched by careful and slow addition of 4N HCl aqueous solution (75 mL). The organic layer was separated, washed with saturated sodium bicarbonate solution (75 mL) and dried over anhydrous magnesium sulfate. The solvent was removed by concentration under reduced pressure to afford the target product 2-(1H-pyrrol-1-yl)benzylethanol (16.8 g, 97 mmol) as a pale yellow oil in 94% yield. Thin layer chromatography (TLC) showed Rf = 0.56 (Expander: dichloromethane/methanol = 97:3).

References

[1] Patent: EP1586559, 2005, A1. Location in patent: Page/Page column 64-65

[2-(1H-PYRROL-1-YL)PHENYL]METHANOL Preparation Products And Raw materials

Raw materials

Preparation Products

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[2-(1H-PYRROL-1-YL)PHENYL]METHANOL Suppliers

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61034-86-4, [2-(1H-PYRROL-1-YL)PHENYL]METHANOLRelated Search:


  • [2-(1H-PYRROL-1-YL)PHENYL]METHANOL
  • 2-(1H-PYRROL-1-YL)BENZYL ALCOHOL
  • (2-PYRROL-1-YL-PHENYL)-METHANOL
  • 2-(1H-Pyrrol-1-yl)benzyl alcohol 97%
  • 4-Hydroxy-3-Methyl-1H-quinolin-2-one
  • [2-(1H-Pyrrol-1-yl)phenyl]methanol 97%
  • 2-(1H-Pyrrol-1-yl)benzyl alcohol, 1-[2-(Hydroxymethyl)phenyl]-1H-pyrrole
  • [2-(1H-Pyrrol-1-yl)phenyl]methanol97%
  • (2-pyrrol-1-ylphenyl)methano
  • Benzenemethanol, 2-(1H-pyrrol-1-yl)-
  • 2-(Pyrrol-1-yl)benzyl Alcohol
  • 61034-86-4